GCMS analysis report, sample AE04419, April 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\MAR2102\4419.D Vial: 10 Acq On : 21 Mar 2002 8:09 pm Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.137 333 337 346 rBV 133678 313687 6.97% 1.390% 2 8.238 346 348 364 rVB 16449 57831 1.29% 0.256% 3 12.269 781 787 804 rVB 1291752 3067109 68.17% 13.591% 4 15.904 1177 1183 1201 rBV 2010141 4115106 91.47% 18.234% 5 21.219 1755 1762 1776 rBV 2062406 4499101 100.00% 19.936%

6 25.663 2239 2246 2255 rBV 2076696 4384091 97.44% 19.426% 7 30.730 2793 2798 2805 rBV 184564 347275 7.72% 1.539% 8 33.723 3117 3124 3141 rBV 1420590 3252664 72.30% 14.413% 9 37.395 3518 3524 3534 rBV2 14214 52836 1.17% 0.234% 10 37.973 3578 3587 3601 rBV2 777699 2363951 52.54% 10.475%

11 38.855 3675 3683 3689 rBV3 14714 58309 1.30% 0.258% 12 40.626 3867 3876 3887 rBV5 11145 55907 1.24% 0.248%

Sum of corrected areas: 22567867

4419.D GCMS0308.M Fri Mar 22 09:41:32 2002

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