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GCMS analysis report, sample AE04508, April 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry results for sample AE04508 analyzed on April 4, 2002.

NYC-WTC_000012391–000012401

Folder label: “GCMS X 3-1-02 A 3-21-02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\MAR2102\4508.D Vial: 15 Acq On : 22 Mar 2002 1:06 am Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.137 333 337 345 rBV 165871 368430 7.47% 1.470% 2 8.238 345 348 356 rVB 24895 60779 1.23% 0.242% 3 12.268 781 787 811 rVB 1485505 3452983 70.02% 13.773% 4 15.904 1177 1183 1200 rBV 2258266 4588723 93.05% 18.303% 5 21.219 1755 1762 1772 rBV 2398933 4931604 100.00% 19.671%

6 25.662 2239 2246 2257 rBV2 2296241 4897038 99.30% 19.533% 7 25.800 2257 2261 2271 rVB 19661 55027 1.12% 0.219% 8 30.730 2793 2798 2804 rBV 195951 389598 7.90% 1.554% 9 33.722 3116 3124 3141 rBV2 1549233 3624684 73.50% 14.458% 10 37.982 3578 3588 3610 rBV2 862675 2702173 54.79% 10.778%

Sum of corrected areas: 25071039

4508.D GCMS0308.M Fri Mar 22 09:45:45 2002

NYC-WTC_000012396

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NYC-WTC_000012396Source: NYC Law Department, mirrored locally

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