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GCMS reanalysis comment for sample AE02565, March 2002

Machine-extracted title · confidence 90%

Laboratory note documenting the re-extraction and re-analysis of sample AE02565 due to low recovery rates.

NYC-WTC_000038773–000038783

Folder label: “GCMS X 3/4/02 A 3/20/02

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Scanned page image, NYC-WTC_000038778
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LSC Area percent Report

Data File : C:\HPCHEM\l\DATA\MAR1902\2565.D Vial: 21 Acq On : 21 Mar 2002 12:43 am Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.151 334 338 347 rBV 23311 53899 1.45% 0.294% 2 12.264 781 786 806 rVB 1084024 2555482 68.56% 13.955% 3 14.862 1064 1069 1076 rVB 140310 263538 7.07% 1.439% 4 15.909 1176 1183 1200 rBV 1582995 3399048 91.19% 18.562% 5 21.215 1754 1761 1781 rBV 1784919 3727231 100.00% 20.354%

6 25.658 2238 2245 2257 rBV2 1731295 3551736 95.29% 19.396% 7 28.899 2593 2598 2609 rBV 53018 117945 3.16% 0.644% 8 30.735 2792 2798 2806 rBV 221450 433733 11.64% 2.369% 9 33.719 3116 3123 3136 rBV2 1078216 2443192 65.55% 13.342% 10 37.969 3578 3586 3608 rBV2 589997 1765898 47.38% 9.644%

Sum of corrected areas: 18311702

2565.D GCMS0308.M Thu Mar 21 14:18:50 2002

NYC-WTC_000038778

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NYC-WTC_000038778Source: NYC Law Department, mirrored locally

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