GCMS analysis results, sample AE04947, April 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\MAR3002\4947.D Vial: 14 Acq On : 30 Mar 2002 3:51 am Operator: Sample : gc/ms scan 3/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title■ : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.249 779 785 799 rBV 1019044 2493529 69.89% 14.835% 2 14.847 1063 1068 1075 rVB 170594 327044 9.17% 1.946% 3 15.884 1175 1181 1197 rBV 1536451 3190985 89.44% 18.985% 4 21.190 1753 1759 1774 rBV 1750956 3567583 100.00% 21.225% 5 25.633 2237 2243 2255 rBV2 1551445 3306214 92.67% 19.670%

6 30.710 279.1 2796 2802 rBV 206039 402210 11.27% 2.393% 7 33.694 3114 3121 3136 rBV 838713 1916877 53.73% 11.405% 8 36.136 3382 3387 3392 rBV 17886 47080 1.32% 0.280% 9 37.375 3515 3522 3528 rBV2 23509 78531 2.20% 0.467% 10 37.935 3575 3583 3599 rBV2 449539 1339943 37.56% 7.972%

11 38.826 3671 3680 3689 rBV 21203 86189 2.42% 0.513% 12 40.579 3863 3871 3882 rBV5 10749 51887 1.45% 0.309%

Sum of corrected areas: 16808072

4947.D GCMS0308.M Tue Apr 02 11:10:03 2002

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