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GCMS quantitation results for sample AE04029, March 2002

Machine-extracted title · confidence 95%

Quantitation report listing response data for deuterated internal standards and surrogates from a March 29, 2002 analysis.

NYC-WTC_000038521–000038531

Folder label: “GCMS X 2/25/02 A 3/23/02

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NYC 9/11 Public Portal Document LSC Area percent Report

Data File : C:\HPCHEM\1\DATA\MAR2202\4029.D Vial: 35 * Acq On : 24 Mar 2002 3:38 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.142 333 337 348 rBV 89212 205079 6.32% 1.240% 2 12.263 781 786 798 rVB 915890 2060241 63.45% 12.458% 3 14.862 1064 1069 1078 rVB 63079 117659 3.62% 0.711% 4 15.899 1176 1182 1200 rBV 1392746 2897669 89.23% 17.522% 5 21.095 1744 1748 1754 rBV 19828 37074 1.14% 0.224%

6 21.214 1754 1761 1779 rBV 1525435 3247256 100.00% 19.636% 7 25.658 2238 2245 2257 rBV 1514656 3198763 98.51% 19.343% 8 '30.734 2792 2798 2807 rVB 185819 377083 11.61% 2.280% 9 33.718 3116 3123 3142 rBV2 1109509 2494165 76.81% 15.082% 10 33.929 3142 3146 3154 rVB 43203 92317 2.84% 0.558%,.

11 37.968 3578 3586 3606 rBV2 582873 1810117 55.74% 10.946%

Sum of corrected areas: 16537423

4029.D GCMS0308.M Tue Mar 26 10:42:39 2002

NYC-WTC_000038526

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NYC-WTC_000038526Source: NYC Law Department, mirrored locally

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