GCMS analysis results for sample AD31591, Feb 28 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\FEB2102\31591.D Vial: 38 Acq On : 23 Feb 2002 3:36 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.204 33 9 344 349 rBV 111155 247537 11.28% 2.171% 2 8.259 349 350 358 rVB 28311 37019 1.69% 0.325% 3 12.326 788 793 807 rVB 625467 1572499 71.67% 13.793% 4 15.971 1184 1190 1202 rBV 976358 2054413 93.64% 18.020% 5 21.286 1763 1769 1785 rBV 1063409 2194037 100.00% 19.244%

6 25.380 2210 2215 2220 rVB2 11454 24610 1.12% 0.216% 7 25.738 2247 2254 2265 rBV2 944194 2067723 94.24% 18.136% 8 30.815 2801 2807 2813 rBV 147099 294562 13.43% 2.584% 9 31.311 2855 2861 2871 rBV 29395 72526 3.31% 0.636%' 10 33.799 3126 3132 3151 rBV2 656389 1577818 71.91% 13.839%

11 34.010 3151 3155 3168 rVB2 8881 30358 1.38% 0.266% 12 38.086 3590 3599 3617 rBV2 386829 1227928 55.97% 10.770%

Sum of corrected areas: 11401030

31591.D GCMS0208,M Wed Feb 27 12:05:48 2002

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