GCMS analysis results for sample AE01441, Mar 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\FEB21021441.D Vial: 13 Acq On : 22 Feb 2002 1:55 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.204 340 344 352 rBV 14521 33708 1.53% 0.304% 2 8.360 356 361 367 rVB 11378 23507 1.06% 0.212% 3 12.335 788 794 808 rVB 656445 1596791 72.33% 14.400% 4 12.565 814 819 824 rBV 13921 31924 1.45% 0.288% 5 15.970 1184 1190 1207 rBV 1014068 2105145 95.36% 18.984%

6 21.286 1763 1769 1782 rBV 1072553 2207515 100.00% 19.907% 7 25.738 2247 2254 2265 rBV2 984610 2093318 94.83% 18.878% 8 30.815 2802 2807 2813 rVB 118178 239753 10.86% 2.162% 9 33.799 3126 3132 3146 rBV2 657918 1539986 69.76% 13.888% 10 36.277 3397 3402 3413 rBV2 16075 53064 2.40% 0.479%

11 38.077 3590 3598 3612 rBV2 369362 1164205 52.74% 10.499%

Sum of corrected areas: 11088916

1441.D GCMS0208.M Fri Feb 22 09:35:27 2002

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