GCMS surrogate recovery results, sample AE00940, March 4, 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\FEB2102\940.D Vial: 62 Acq On : 24 Feb 2002 5:08 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.197 340 344 358 rBV 65028 165207 9.19% 1.751% 2 12.329 789 794 808 rVB 564783 1342477 74.69% 14.227% 3 14.927 1071 1077 1083 rVB 65981 131080 7.29% 1.389% 4 15.973 1185 1191 1202 rBV 815424 1731372 96.32% 18.349% 5 21.279 1763 1769 1789 rBV 832395 1797447 100.00% 19.049%

6 22.757 1923 1930 1935 rBV 24160 48163 2.68% 0.510% 7 25.732 2247 2254 2265 rBV2 818954 1729650 96.23% 18.331% 8 30.809 2802 2807 2814 rVB 134948 263001 14.63% 2.787% 9 33.801 3126 3133 3152 rBV 555149 1289243 71.73% 13.663% 10 38.079 3590 3599 3617 rBV 300937 938235 52.20% 9.943%

Sum of corrected areas: 9435875

940.D GCMS0208.M Fri Mar 01 09:10:55 2002

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