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GCMS analysis results for sample AE03834, Mar 18 2002

Machine-extracted title · confidence 50%

Laboratory report documenting GCMS analysis of sample AE03834 for unknown compounds on March 18, 2002.

NYC-WTC_000038364–000038374

Folder label: “GCMS X 2/22/02 A 2/24/02

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Scanned page image, NYC-WTC_000038368
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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\FEB2102\3834.D Vial: 74 Acq On : 24 Feb 2002 6:51 pm Operator: .Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 8.198 340 344 358 rBV 101903 253448 12.65% 2.507% 2 8.354 358 361 369 rVB 8036 21218 1.06% 0.210% 3 9.262 456 460 472 rBV 44005 107623 5.37% 1.065% 4 12.329 789 794 808 rVB 615415 1426631 71.19% 14.113% 5 15.973 1185 1191 1209 rVB 885495 1848969 92.26% 18.291%

6 21.289 1763 1770 1787 rBV 921201 2004012 100.00% 19.825% 7 25.732 2247 2254 2266 rBV2 868869 1840538 91.84% 18.208% X 8 30.809 2802 2807 2814 rBV 132081 260754 13.01% 2.580% 9 33.801 3126 3133 3153 rBV 591925 1363398 68.03% 13.488% 10 38.079 3591 3599 3620 rBV2 316991 982012 49.00% 9.715%,

Sum of corrected areas: 10108603

3834.D GCMS0208.M Wed Mar 13 11:33:38 2002

NYC-WTC_000038368

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NYC-WTC_000038368Source: NYC Law Department, mirrored locally

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