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GCMS analysis results for sample AE03915, Mar 18 2002

Machine-extracted title · confidence 50%

Laboratory report documenting GCMS analysis of sample AE03915 for unknown compounds on March 18, 2002.

NYC-WTC_000038342–000038351

Folder label: “GCMS X 2/22/02 A 2/24/02

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Scanned page image, NYC-WTC_000038347
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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C: \HPCHEM\1\DATA\FEB2102\3915.D Vial: 77 Acq On : 24 Feb 2002 9:47 pm Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering-. 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.197 340 344 359 rBV 77766 225248 14.62% 2.885% 2 12.328 789 794 811 rVB 431042 1092985 70.95% 13.997% 3 15.973 1185 1191 1209 rBV 681617 1437635 93.32% 18.411% 4 21.279 1763 1769 1791 rBV 726867 1540606 100.00% 19.730% 5 25.731 2247 2254 2265 rBV2 673280 1429238 -92.77% 18.304%

6 25.869 2265 2269 2278 rVB2 5618 16135 1.05% 0.207% 7 30.808 2802 2807 2814 rVB 109011 203876 13.23% 2.611% 8 33.801 3126 3133 3146 rBV2 453263 1078644 70.01% 13.814% 9 38.070 3591 3598 3616 rBV2 239961 784145 50.90% 10.042%

Sum of corrected areas: 7808512

3915.D GCMS0208.M Wed Mar 13 11:36:47 2002

NYC-WTC_000038347

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NYC-WTC_000038347Source: NYC Law Department, mirrored locally

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