GCMS analysis results, sample AE02785, March 2002

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\MAR0102\2785.D Vial: 19 Acq On 2 Mar 2002 2:03 am Operator: Sample gc/ms scan 2/6 Inst : GC/MS 2 09 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.316 786 792 807 rVB 828857 1916918 68.59% 12.109% 2 15.951 1182 1188 1205 rBV 1147693 2560772 91.63% 16.176% 3 21.266 1761 1767 1792 rBV 1281139 2794605 100.00% 17.653% 4 25.719 2245 2252 2263 rBV2 1181371 2695942 96.47% 17.030% 5 25.847 2263 2266 2273 rVB 11057 30145 1.08% 0.190%

6 27.683 2461 2466 2475 rBV 13561 29104 1.04% 0.184% 7 30.786 2799 2804 2812 rBV 149589 319120 11.42% 2.016% 8 32.320 2965 2971 2979 rBV 19525 50886 1.82% 0.321% 9 33.311 3074 3079 3086 rBV 28076 72545 2.60% 0.458% 10 33.779 3123 3130 3150 rBV2 878147 2176493 77.88% 13 .749%

11 34.266 3177 3183 3197 rBV2 41351 122444 4.38% 0.773% 12 35.193 3279 3284 3301 rBV 57270 169235 6.06% 1.069% 13 36.074 3375 3380 3394 rBV 87894 265655 9.51% 1.678% 14 36.992 3474 3480 3494 rBV 100787 339292 12.14% 2.143% 15 38.057 3584 3596 3617 rBV2 599083 2065746 73.92% 13.049%

16 39.223 3716 3723 3742 rBV2 29616 164668 5.89% 1.040% 17 40.609 3867 3874 3885 rBV5 10165 56755 2.03% 0.359%

Sum of corrected areas: 15830325

2785.D GCMS0208.M Tue Mar 05 10:50:13 2002

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