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GCMS analysis results for sample AE02604, Mar 15, 2002

Machine-extracted title · confidence 90%

Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.

NYC-WTC_000005394–000005414

Folder label: “GCMS X 2/5/02 A 3/7/02

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Scanned page image, NYC-WTC_000005399
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NYC 9/11 Public Portal Document LSC Area Percent Report

• Data File C:\HPCHEM\1\DATA\MAR0702\2604.D Vial: 17 Acq On 8 Mar 2002 5:28 am Operator: Sample gc/ms scan 2/5 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.192 338 343 354 rBV2 13842 54101 1.36% 0.237% 2 12.305 784 791 803 rBV 1050463 2714950 68.43% 11.917% 3 14.894 1068 1073 1078 rBV 42829 80292 2.02% 0.352% 4 15.940 1180 1187 1199 rBV 1720642 3611083 91.01% 15.851% 5 18.052 1412 1417 1423 rVB 108276 209748 5.29% 0.921%

6 20.889 1720 1726 1732 rBV 83887 157577 3.97% 0.692% 7 21.247 1758 1765 1775 rBV 1878042 3884291 97.90% 17.050% 8 21.651 1803 1809 1821 rVB 35634 71470 1.80% 0.314% 9 23.413 1995 2001 2006 rBV 58119 111446 2.81% 0.489% 10 25.589 2231 2238 2242 rBV2 43419 85836 2.16% 0.377%

11 25.690 2242 2249 2260 rBV2 1781526 3967610 100.00% 17.416% 12 25.828 2260 2264 2275 rVB 16035 42688 1.08% 0.187% 13 27.517 2441 2448 2455 rVB 31993 61599 1.55% 0.270% 14 29.289 2635 2641 2646 rVB 25195 51920 1.31% 0.228% 15 30.767 2797 2802 2807 rBV 225247 443762 11.18% 1.948%

16 30.886 2809 2815 2822 rVB 25893 57917 1.46% 0.254% 17 32.346 2967 2974 2982 rBV2 22507 53754 1.35% 0.236% 18 33.759 3117 3128 3145 rBV2 1629921 3805935 95.93% 16.706% 19 34.999 3257 3263 3276 rBV2 15503 46041 1.16% 0.202% 20 38.028 3580 3593 3612 rBV2 1037688 3269771 82.41% 14.353%

Sum of corrected areas: 22781791

2604 .D GCMS0208.M Wed Mar 13 14:50:17 2002

NYC-WTC_000005399

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NYC-WTC_000005399Source: NYC Law Department, mirrored locally

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