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GCMS analysis results for sample AE06449, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.

NYC-WTC_000039497–000039521

Folder label: “GCMS X 3/19/02 A 4/17/02

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Scanned page image, NYC-WTC_000039502
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\APR1702\6449.D Vial: 7 Acq On : 17 Apr 2002 2:06 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.096 328 332 343 rBV 150702 382656 10.35% 1.944% 2 11.612 711 715 725 rBV 18602 46204 1.25% 0.235% 3 12.209 775 780 801 rVB 1097982 2598539 70.28% 13.202% 4 14.807 1059 1063 1070 rVB 106896 210324 5.69% 1.069% 5 15.844 1170 1176 1193 rBV 1624798 3269454 88.43% 16.611%

6 17.965 1402 1407 1417 rVB 168578 326690 8.84% 1.660% 7 18.681 1480 1485 1490 rBV 85679 148897 4.03% 0.756% 8 20.802 1710 1716 1726 rBV 137019 258160 6.98% 1.312% 9 21.151 1747 1754 1777 rBV 1765215 3697391 100.00% 18.785% 10 21.564 1792 1799 1803 rBV 45685 79774 2.16% 0.405%

11 23.326 1985 1991 1996 rBV 111971 219818 5.95% 1.117% 12 25.493 2222 2227 2231 rBV 88903 163815 4.43% 0.832% 13 25.585 2231 2237 2249 rW2 1631370 3445620 93.19% 17.506% 14 27.430 2432 2438 2442 rBV 55406 111787 3.02% 0.568% 15 29.193 2624 2630 2636 rBV 41403 84439 2.28% 0.429%

16 30.661 2785 2790 2796 rBV 224637 425633 11.51% 2.162% 17 30.781 2798 2803 2810 rVB 39258 77444 2.09% 0.393% 18 32.240 2955 2962 2968 rBV2 33021 74021 2.00% 0.376% 19 33.645 3105 3115 3130 rBV 936928 2264061 61.23% 11.503% 20 34.894 3246 3251 3257 rBV 25730 59877 1.62% 0.304%

21 36.087 3375 3381 3389 rBV 26511 66783 1.81% 0.339% 22 37.317 3507 3515 3528 rBV2 20673 67619 1.83% 0.344% 23 37.868 3567 3575 3590 rBV2 536272 1549722 41.91% 7.873% 24 38.749 3664 3671 3681 rVB2 15237 54143 1.46% 0.275%

Sum of corrected areas: 19682871

6449.D GCMS0412.M Thu Apr 18 09:10:39 2002

NYC-WTC_000039502

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NYC-WTC_000039502Source: NYC Law Department, mirrored locally

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