GCMS reference data sample AE12152, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY2402\REF2 .D Vial: 5 Acq On : 24 May 2002 7:28 pm Operator: Morgan Sample : gc/ms scan 5/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 28 11:42 2002 Quant Results File: GCMS0520 .RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 11:39:13 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 12.14 152 547482 40.00 ug/1 0.00 10) Naphthalene-d8 15.78 136 2175643 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.08 164 1045681 40.00 ug/1 0.00 30) Phenanthrene-diO 25.53 188 1517386 40.00 ug/1 0.00 38) Chrysene-dl2 33.58 240 826044 40,00 ug/1 -0.03 44) Perylene-dl2 37.79 264 553634 40.00 ug/1 -0.01

System Monitoring Compounds 28) TCMX 23.22 209 180417 34.33 ug/L -0.01 Spiked Amount 40.000 Recovery 85.82%

Target Compounds Qvalue 2) N-nitrosodimethylamine 5.79 74 143292 8.72 ug/1 82 3) bis(2-Chloroethyl)ether 11.54 93 279832 12.85 ug/1 94 4) 1,3-Dichlorobenzene 12.04 146 247025 14.02 ug/1 98 5) 1,4-Dichlorobenzene 12.19 146 259820 13.46 ug/1 99 6) 1,2-Dichlorobenzene 12.70 146 254976 15.25 ug/1 99 7) 2,2’-oxybis(1-Chloropropan 13.02 45 454826 9.23 ug/1 # 93 8) N-Nitrosodi-n-propylamine . 13.41 70 190090 12.30 ug/1 # 85 9) Hexachloroethane 13.55 117 77865 9.45 ug/1 93 11) Nitrobenzene 13.82 77 244336 12.92 ug/1 # 87 12) Isophorone 14.47 82 544139 14.53 ug/1 +: 94 13) bis (2-Chloroethoxy) methane 15.16 93 329082 13.11 ug/1 # 98 14) 1,2,4-Trichlorobenzene 15.67 180 209519 15.42 ug/1 99 15) Naphthalene 15.83 128 811523 16.52 ug/1 98 16) Hexachiorobutadiene 16.38 225 62599 9.52 ug/1 98 18) Hexachlorocyclopentadiene 18.58 237 16432 3.88 ug/1 96 19) 2-Chioronaphthalene 19.34 162 417382 17.91 ug/1 96 20) Dimethylphthalate 20.43 163 484272 16.51 ug/1 99 21) 2,6-Dinitrotoluene 20.65 165 97385 15.95 ug/1 # 89 2 2) Acenaphthylene 20.61 152 633309 14.83 ug/1 97 2 3) Acenaphthene 21.17 153 432572 16.95 ug/1 100 24) 2,4-Dinitrotoluene 21.82 ‘ 165 114818 17.15 ug/1 # 84 25) Diethylphthalate 22.57 149 485595 17.91 ug/1 100 26) 4-Chlorophenylphenylether 22.72 204 215557 15.91 ug/1 97 27) Fluorene 22.70 166 468744 18.12 ug/1 99 29) Azobenzene 23.18 77 484003 12.39 ug/L # 89 31) N-Nitrosodiphenylamine 23.11 168 169784 16.98 ug/1 # 83 32) 4-Bromophenylphenylether 24.18 248 105062 13.26 ug/1 95 33) Hexachlorobenzene 24.62 284 123668 14.55 ug/1 # 93 34) Phenanthrene 25.59 178 631990 17.27 ug/1 100 (#) = qualifier out of range (m) = manual integration REF2.D GCMS0520.M Tue May 28 11:44:29 2002 Page 1

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