GCMS calibration data sample AE12152, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAY24 02\CAL2 0.D Vial: 2 Acq On 24 May 2002 4:31 pm Operator: Morgan Sample Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 28 11:36 2002 Quant Results File: GCMS0520 .RES *e- Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 11:36:11 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.14 152 433349 40.00 ug/1 0.00 10) Naphtha1ene-d8 15.77 136 1697708 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.08 164 819824 40.00 ug/1 0.00 30) Phenanthrene-diO 25.52 188 1177906 40.00 ug/1 0.00 3.8) Chrysene-dl2 33.58 240 620231 40.00 ug/1 -0.03 44) Perylene-dl2 37.79 264 403518 40.00 ug/1 -0.01 System Monitoring Compounds 28) TCMX 23.22 209 44994 43.68 ug/L -0.01 Spiked Amount 40.000 Recovery = 109.20% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.79 74 200655 15.42 ug/1 82 3) bis(2-Chloroethyl)ether 11.54 93 286066 16.60 ug/1 90 4) 1,3-Dichlorobenzene 12.04 146 286586 20.55 ug/1 96 5) 1,4-Dichlorobenzene 12.19 146 313384 20.51 ug/1 99 6) 1,2-Dichlorobenzene 12.70 146 273697 20.67 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.03 45 425534 10.92 ug/1 # 92 8) N-Nitrosodi-n-propylamine 13.41 70 189949 15.52 ug/1 # 87 9) Hexachloroethane 13.55 117 124087 19.02 ug/1 93 11) Nitrobenzene 13.82 77 245480 16.64 ug/1 +i 89 12) 1sophorone 14.47 82 484487 16.58 ug/1 +i . 93 13) bis(2-Chloroethoxy)methane 15.16 93 323680 16.53 ug/1 # 96 14) 1,2,4-Trichlorobenzene 15.66 180 234639 22.13 ug/1 99 15) Naphthalene 15.84 128 786612 20.52 ug/1 98 16) Hexachlorobutadiene 16.38 225 97248 18.95 ug/1 99 18.) Hexachlorocyclopentadiene 18.57 237 56351 16.95 ug/1 99 19) 2-Chloronaphthalene 19.34 162 371676 20.34 ug/1 96 20) Dimethylphthalate 20.43 163 468569 20.37 ug/1 99 21) 2,6-Dinitrotoluene 20.65 165 95351 19.91 ug/1 90 2 2) Acenaphthylene 20.61 152 664400 19.84 ug/1 98 23) Acenaphthene 21.17 153 405879 20.29 ug/1 99 24) 2,4-Dinitrotoluene 21.82 165 99580 18.97 ug/1 # 84 25) Diethylphthalate 22.57 149 430937 20.28 ug/1 100 26) 4-Chlorophenylphenylether 22.72 204 205959 19.39 ug/1 95 27) Fluorene 22.70 166 429027 21.15 ug/1 99 29) Azobenzene 23.18 77 493849 16.13 ug/L # 91 31) N-Nitrosodiphenylamine 23.11 168 166997 21.51 ug/1 # 84 32) 4-Bromophenylphenylether 24.18 248 103090 16.76 ug/1 96 33) Hexachlorobenzene 24.62 284 114027 17.28 ug/1 # 90 34) Phenanthrene 25.59 178 607475 21.39 ug/1 100 (#) = qualifier out of range (m) = manual integration CAL20.D GCMS0520.M Tue May 28 11:38:46 2002 Page 1

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