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Document / 4 pages

GCMS calibration data sample AE12152, May 2002

Machine-extracted title · confidence 90%

Calibration report for GCMS analysis of sample AE12152 listing various organic compounds and detection limits.

NYC-WTC_000013321–000013324

Folder label: “GCMS X 5/22/02 A 5/25/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File C:\HPCHEM\l\DATA\MAY2402\CAL20.D Vial: 2 Acq On 24 May 2002 4:31 pm Operator: Morgan Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 28 11:36 2002 Quant Results File: GCMS0520.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 11:36:11 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.72 178 602198 20.61 ug/1 99 36) Di-n-butylphthalate 27.50 149 743850 19.24 ug/1 99 37) Fluoranthene 29.21 202 560841 19.51 ug/1 100 39) Pyrene 29.89 202 526576 23.15 ug/1 94 40) Butylbenzylphthalate 32.02 149 234787 20.21 ug/1 92 41) Benzo(a)anthracene 33.52 228 . 328785 19.37 ug/1 98 42) Bis(2-ethylhexyl)phthalate 33.81 149 307984 20.16 ug/1 # 97 43) Chrysene 33.65 228 351547 20.97 ug/1 98 45) Di-n-Octylphthalate 35.55 149 387851 16.61 ug/1 # 91 46) Benzo(b)fluoranthene 36.62 252 , 266590 17.73 ug/1 97 47) Benzo(k)fluoranthene 36.69 252 302631 19.45 ug/1 96 48) Benzo(a)pyrene 37.60 252 258225 18.50 ug/1 97 49) Indeno(1,2,3-cd)pyrene 41.83 276 241593 18.00 ug/1 95 50) Dibenz(a,h)anthracene 41.90 278 189299 17.66 ug/1 96 51) Benzo(g,h,i)perylene 43.03 276 200208 18.67 ug/1 94

(#) = qualifier out of range (m) = manual integration CAL20.D GCMS0520.M Tue May 28 11:38:46 2002 Page 2

NYC-WTC_000013323

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NYC-WTC_000013323Source: NYC Law Department, mirrored locally

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