GCMS reference data for sample AE12278, May 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAY2902\REFA2.D Vial: 18 Acq On : 30 May 2002 4:01 am Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 30 9:59 2002 Quant Results File: GCMS0528.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 08:55:48 2002 Response via : Initial Calibration DataAcq Meth : GCMS0528

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.07 152 626032 40.00 ug/1 -0.08 10) Naphthalene-d8 15.69 136 2526355 40.00 ug/1 -0.10 17) Acenaphthene-diO 20.99 164 1216324 40.00 ug/1 -0.10 30) Phenanthrene-diO 25.43 188 1891416 40.00 ug/1 -0.10 38) Chrysene-dl2 33.48 240 1179430 40.00 ug/1 -0.12 44) Perylene-dl2 37.65 264 743514 40.00 ug/1 -0.15

System Monitoring Compounds 28) TCMX 23.14 209 260713 31.05 ug/L -0.10 Spiked Amount 40.000 Recovery 77.63% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.72 74 186183 9.91 ug/1 83 3) bis(2-Chloroethyl)ether 11.47 93 374961 15.06 ug/1 93 4) 1,3-Dichlorobenzene 11.97 146 266994 13.25 ug/1 99 5) 1,4-Dichlorobenzene 12.11 146 290007 13.14 ug/1 99 6) 1,2-Dichlorobenzene 12.63 146 290983 15.22 ug/1 99 7) 2,2'-oxybis(1-Chioropropan 12.95 45 620367 11.02 ug/1 # 93 8) N-Nitrosodi-n-propylamine 13.33 70 261463 14.79 ug/1 # 86 9) Hexachloroethane 13.47 117 77717 8.25 ug/1 98 11) Nitrobenzene 13.75 77 349045 15.90 ug/1 # 87 12) 1sophorone 14.40 82 753329 17.33 ug/1 i- 93 13) bis(2-Chloroethoxy)methane 15.08 93 451473 15.49 ug/1 # 98 14) 1,2,4-Trichlorobenzene 15.58 180 246425 15.62 ug/1 99 15) Naphthalene 15.75 128 1059720 18.58 ug/1. # 81 16) Hexachlorobutadiene 16.30 225 67726 8.87 ug/1 98 18) Hexachlorocyclopentadiene 18.49 237 9776 1.98 ug/1 99 19) 2-Chioronaphthalene 19.25 162 549131 20.25 ug/1 96 20) Dimethylphthalate 20.35 163 693767 20.33 ug/1 99 21) 2,6-Dinitrotoluene 20.56 165 137216 19.32 ug/1 93 22) Acenaphthylene 20.52 152 861605 17.35 ug/1 98 2 3) Acenaphthene 21.08 153 593378 19.99 ug/1 99 24) 2,4-Dinitrotoluene 21.72 165 170891 21.95 ug/1 # 88 25) Diethylphthalate 22.49 149 710503 22.53 ug/1 99 26) 4-Chlorophenylphenylether 22.63 204 302918 19.22 ug/1 99 2 7) Fluorene 22.61 166 650847 21.63 ug/1 99 29) Azobenzene 23.09 77 710910 15.65 ug/L # 92 31) N-Nitrosodiphenylamine 23.02 168 194983 15.64 ug/1 # 86 32) 4-Bromophenylphenylether 24.09 248 155263 15.72 ug/1 93 3 3) Hexachlorobenzene 24.52 284 182262 17.21 ug/1 94 34) Phenanthrene 25.50 178 927741 20.34 ug/1 99

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS0528.M Thu May 30 10:00:37 2002 Page 1

NYC-WTC_000013717