GCMS reference data for sample AE12278, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAY29O2\REFA1.D Vial: 17 Acq On : 30 May 2002 3:03 am Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 30 9:46 2002 Quant Results File: GCMS0528.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 08:55:48 2002 Response via : Initial Calibration DataAcq Meth : GCMS0528

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 12.07 152 598339 40.00 ug/1 -0.08 10) Naphthalene-d8 15.69 136 2437964 40.00 ug/1 -0.10 17) Acenaphthene-diO 20.99 164 1184186 40.00 ug/1 -0.10 3 0) Phenanthrene-dl0 25.42 188 1840385 40.00 ug/1 -0.11 38) Chrysene-dl2 33.48 240 1147751 40.00 ug/1 -0.13 44) Perylene-dl2 37.66 264 727789 40.00 ug/1 -0.14 System Monitoring Compounds 28) TCMX 23.14 209 253007 30.95 ug/L -0.09 Spiked Amount 40.000 Recovery 77.38% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.73 74 187694 10.45 ug/1 80 3) bis(2-Chloroethyl)ether 11.47 93 376566 15.83 ug/1 93 4) 1,3-Dichlorobenzene 11.97 146 287709 14.94 ug/1 100 5) 1,4-Dichlorobenzene 12.11 146 307565 14.58 ug/1 99 6) 1,2-Dichlorobenzene 12.63 146 306502 16.77 ug/1 100 7) 2,2'-oxybi s(1-Chioropropan 12.95 45 621539 11.55 ug/1 # 93 8) N-Nitrosodi-n-propylamine 13.33 70 259248 15.34 ug/1 # 85 9) Hexachloroethane 13.47 117 88489 9.82 ug/1 98 11) Nitrobenzene 13.75 77 339224 16.01 ug/1 # 86 12) 1sophorone 14.40 82 742821 17.70 ug/1 # 94 13) bis(2-Chloroethoxy)methane 15.08 93 449332 15.98 ug/1 99 14) 1,2,4-Trichlorobenzene 15.58 180 255414 16.77 ug/1 98 15) Naphthalene 15.75 128 1065923 19.36 ug/1 # 81 16) Hexachlorobutadiene 16.30 225 81556 11.07 ug/1 98 18) Hexachlorocyclopentadiene 18.49 237 11830 2.46 ug/1 95 19) 2-Chloronaphthalene 19.25 162 551334 20.89 ug/1 96 20) Dimethylphthalate 20.35 163 671352 20.21 ug/1 100 21) 2,6-Dinitrotoluene 20.56 165 132414 19.15 ug/1 96 22) Acenaphthylene 20.52 152 859001 17.76 ug/1 97 23) Acenaphthene 21.08 153 583686 20.20 ug/1 99 24) 2,4-Dinitrotoluene 21.72 165 160356 21.15 ug/1 89 25) Diethylphthalate 22.48 149 679798 22.14 ug/1 98 26) 4-Chlorophenylphenylether 22.63 204 300916 19.61 ug/1 100 27) Fluorene 22.61 166 639106 21.82 ug/1 99 29) Azobenzene 23.09 77 692636 15.66 ug/L 91 31) N-Nitrosodiphenylamine 23.02 168 194772 16.06 ug/1 # 86 32) 4-Bromophenylphenylether 24.09 248 151444 15.76 ug/1 95 33) Hexachlorobenzene 24.52 284 176677 17.14 ug/1 95 34) Phenanthrene 25.49 178 914529 20.61 ug/1 99 (#) = qualifier out of range (m) = manual integration REFA1.D GCMS0528.M Thu May 30 09:58:54 2002 Page 1

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