GCMS pesticide analysis results, sample AE11573, May-June 2002

NYC 9/11 Public Portal Document LLOLaLY bedLci tompouud KepOLt Data’File : C:\MSDCHEM\1\DATA\052902\11311RR.D Vial: 16 •Acq On : 29 May 2002 2:39 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11311 RE-EXTD 5/23/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\052802.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L

Peak Number 9 Tricosane (CAS) $$ n-Tricosane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 21.36 0.08 ug/L 120762 Phenanthrene d-10 22.51 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Tricosane (CAS) $$ n-Tricosane 324 C23H48 000638-67-5 86 2 Hentriacontane 437 C31H64 000630-04-6 78 3 Tetratriacontane $$ n-Tetratriac... 479 C34H70 014167-59-0 78 4 Docosane $$ n-Docosane $$ Normal... 310 C22H46 000629-97-0 78 Abundance Scan 1134 (21.362 min): 11311RR.D (-) m/z 57.10 100.00% 57 85

5000' 113 1141 — 169 Ab 21.00 21.20 21.40 21.60 0- — m/z 71.05 90.85% 1 miz-> 0 50 100 150 200 250 300 350 400 Abundance #275685: Tricosane (CAS) $$ n-Tricosane 57

5000 85 21.00 21.20 21.40 21.60 m/z 85.10 86.45% 28 , 113.. . J J J 1’1 ,169, 211 239 267 295 324 0-,4 T1444**0,4 4 ro4 Pin t tep u** , । t m/z-> 0 50 100 150 200 250 300 350 400 Abundance #349910: Hentriacontane 57

a 21.00 ... . 21.20 21.40 21.60 5000 m/z 99.15 35.81% 85

113 29 J J 1 | 141,169 197 225 253 281 309 351379407 436 0--TTTo—f—mTTT n/z-> 0 50i 100 150 200 250 300 350 400 Abundance #363627: Tetratriacontane $$ n-Tetratriacontane . ............... . 57 21.00 21.20 21.40 21.60 m/z 113.10 33.27%

5000 85

29 . fn/z-> 0- 0 44450 .41001131.17198197,225,253 281 311337, 367, , 410435, 150 200 250 300 350 400 ‘‘ 21.00 21.20 21.40 21.60 1 ■ i •

1311RR.D 052802.M Mon Jun 03 15:50:24 2002 Page 11

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