GCMS pesticide analysis results, sample AE11573, May-June 2002

NYC 9/11 Public Portal Document LLDLcLy btdLCi tompound KepOLC

Data File : C:\MSDCHEM\1\DATA\052902\11311RR.D Vial: 16 : Acq On : 29 May 2002 2:39 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11311 RE-EXTD 5/23/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\052802.M (RTE Integrator) Title : Quantitation For Method 525.2 2** Library : C: \DATABASE\WILEY7N. L ***

Peak Number 8 Hexadecane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

19.96 0.08 ug/L 114038 Acenaphthene-d10 18.19

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Hexadecane 226 C16H34 000544-76-3 94 2 Hexadecane 226 C16H34 000544-76-3 93 3 Hexadecane (CAS) $$ n-Hexadecane... 226 C16H34 000544-76-3 93 4 Hexadecane (CAS) $$ n-Hexadecane... 226 C16H34 000544-76-3 91 Abundance Scan 980 (19.965 min): 11311RR.D (-) m/z 57.10 100.00% 57 71 85 5000

-rwA rYM4nn Ai ,0 AA 7 113 126 141 155169 226 19.6019.8020.00 20.20

miz-> 11 0+ ■ ■ i ■ ■ • ■ i ■ ■ • 20 40 60 UM m/z 71.10 73.60% 80 100 120 140 160 180 200 220 Abundance #154908: Hexadecane 57 43

5000 71

85 AAL MAAPP4 19.60 19.8020.00 20.20 m/z 85.10 54.20% 29 99 113 127 141 155 169 183 197 226 •n/z-> 01 —4-44 hydssdonshyudosgsodgauanpahi 20 40 60 80 100 120 140 160 180 200 220 Abundance #154904: Hexadecane 57 43 71 MAp u_________ i • ■ ■ ■ i ■ ■ ■ • i • 19.60 19.80 20.00 20.20 5000 m/z 55.00 26.04% 85

29 99 0+ ■. A. A. 113 127 141 155 169 183 197... 226 1.1* . ’h > . T > । > i < i p > । । i । | । । i । i rj > . > ■ । । > > m/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #154916: Hexadecane (CAS) $$ n-Hexadecane $$ Cetane $$ n-C... 43 57 MALAAAAAAAAAA 19.60 19.80 20.00 20.20 ~ 71 m/z 69.10 16.56% 85 5000

m/z—> 0 1 ■ I ■ ‘1' 20 40 i TTppmpmpphr 99 113 127 141 155 169 183 197 226 60 ’ 4t 80 J 100 120 140 160 180 200 220 MLA 19.60 19.80 20.00 20.20

1311RR.D 052802.M Mon Jun 03 15:50:23 2002 Page 10

NYC-WTC_000012638