GCMS pesticide analysis results, sample AE11573, May-June 2002

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Data File : C:\MSDCHEM\1\DATA\052902\11311RR.D Vial: 16 : Acq On : 29 May 2002 2:39 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11311 RE-EXTD 5/23/02 Inst : Instrumen Mise Multipir: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\052802.M (RTE Integrator) Title : Quantitation For Method 525.2 2** Library : C:\DATABASE\WILEY7N.L

Peak Number 7 Pentacosane $$ n-Pentacosane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 18.97 0.08 ug/L 118944 Acenaphthene-dl0 18.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Pentacosane $$ n-Pentacosane 352 C25H52 000629-99-2 80 2 Docosane $$ n-Docosane $$ Normal... 310 C22H46 000629-97-0 80 3 Hexadecane 226 C16H34 000544-76-3 72 4 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 72 Abundance Scan 870 (18.967 mln): 11311RR.D (-) m/z 71.10 100.00%

5000

I I 111 I I 1 . I 1, J J I I I 155 NA AWW 18.60 18.80 19.00 19.20 m/z 57.00 73.21% 0- ■ i ■ miz-> 50 100 150 200 250 300 350 Abundance #300501: Pentacosane $$ n-Pentacosane 57

5000 85 erin PT A A P 18.60 18.80 19.00 19.20 m/z 85.10 69.73% 28 1 113 1X1 iii 1141 0- 1,1) f-1 Jill T4I r 169189 211 239 267 295 323 352 t-t-T I *"***41**118* miz-> 50 100 150 200 250 300 350 Abundance #261311: Docosane $$ n-Docosane $3 Normal-docosane 57

85 AAAMMNMA 18.60 18.80 19.00 19.20 m/z 55.05 27.23% 5000

113 0- 37 . 1 r 1 L 1 I /, 171198, 197,225 253 281 31° , n/z-> 50 100 150 200 250 300 350 Abundance #154904: Hexadecane 57 --=AmR 18.60 18.80 19.00 19.20 m/z 111.10 24.97%

5000 85

29

0 —Y BE J A,41134141 - 169, 197226, 1 ‘ i ‘ m/z—> 50 100 ' 150 200 250 ' 300 350

.1311RR.D 052802.M Mon Jun 03 15:50:21 2002 Page 9

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