Water quality monitoring data sheet, May 2002

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Data File : C:\MSDCHEM\1\DATA\051302\11311.D Vial: 13 Acq On : 13 May 2002 9:36 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11311 5/10/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\050802.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L

Peak Number 3 pentadecane Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

14.78 0.08 ug/L 67153 Acenaphthene-dl0 18.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual l pentadecane 212 C15H32 000629-62-9 83 2 Tetradecane (CAS) $$ n-Tetradeca... 198 C14H30 000629-59-4 78 3 Hexadecane 226 C16H34 000544-76-3 72 4 Eicosane 282 C20H42 000112-95-8 72 Abundance Scan 408 (14.777 min): 11311.D (-) m/z 57.10 100.00% 57 71 85

5000

99 113 127 155 psANA 4 14.40 14.60 14.80 15.00 01 i ‘ ■ ■ ■ i ■ ‘ I I I m/z 71.10 97.93% n/z-> :20 40 60 80 100 120 140 160 180 200 220 Abundance #134046: pentadecane 43 57

5000 71 ... A.AA.M 14.40 14.60 14.80 15.00 29 85 m/z 85.20 69.63%

m/z-> 01TTTT mrr r ;20 40 60 4.?.113,127140,155212 80 100 120 140 160 180 200 220 Abundance #113302: Tetradecane (CAS) $$ n-Tetradecane $$ Isotetradecane 43 57 —4 "‘I 14.40 14:60 14.80 15.00 5000 71 m/z 69.10 24.88%

29 85

01 I'111 1 P 1 r TTTT 1.4..9.112 127140.155 ..... m/z-> :20 40 60 80 100 120 140 160 180 200 220 Abundance #154908: Hexadecane 57 43 14.40 14.60 14.80 15.00 T m/z 55.00 23.01% 71 5000 85 29 )

miz—> 0 TId 20 +40 UJ. 60 80 100 120 140 160 180 200 220 14.40 14.60 14.80 15.00

.1311.D 050802.M Tue May 14 11:10:33 2002 Page 5

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