GCMS blank analysis results, March 27, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

* Data File : C:\MSDCHEM\l\DATA\032602\LBB326.D Vial: 26 Acq On : 27 Mar 2002 1:55 am Operator: McLean Sample : LB 3/1/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.05 0.70 ug/L 313250 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 78 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 52 3 Benzeneethanamine, N- [ (pentaf luo. . . 563 C24H34F5NO3Si3 055429-13-5 47 4 Benzoi acid, 2,5-bis(trimethyls... 370 C16H30O4Si3 003618-20-0 47 Abundance Scan 1527 (12.051 min): LBB326.D (-) m/z 73.10 100.00% 73

5000 267 355 TT-p-n-ry-rn- unr 11.80 12.00 12.20 12.40 119154 0- TTnrir * 191 ** 237. w/j 325 m/z- 267.00 36.85% ert?ji ’t4 111. i**i 11 ‘ ■ i ■ ■ ■ ■ i' ■ ■ • i ■ ■ • ■ i ■ • miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 ‘+111111 -MmPp—r 11.80 12.00 12.20 12.40 m/z 355.10 28.59%

207 , 323 0- —mmmer —P PBIImwpummmmT m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 . Mi . 11.80 12.00 12.20 12.40 5000 m/z 356.10 10.53% 267 355

28| । 103133163193223 1 323 0- TTfor TKKmummmmOumuaTT m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #378300: Benzeneethanamine, N-[(pentafluorophenyl)methylen... ----- 73 355 11.80 12.00 12.20 12.40 m/z 74.10 8.95%

5000

„ 41, 117147177207 251281 386 458 548 OTTTfftfng . i |T . r, 1111 Tri । 111 rrTrm I • • ‘41 T iz—> 50 100 150 200 250 300 350 400 450 500 550 11.80 12.00 12.20 12.40

LBB326.D 5080302.M Wed Mar 27 08:59:47 2002 Page 3

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