GCMS analysis report, sample AE04417, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2102\4418.D Vial: 9 Acq On : 21 Mar 2002 7:09 pm Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Sulfur Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

29.33 0.23 ug/1 52545 Phenanthrene-dl 0 25.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Sulfur 256 S8 007704-34- 2 Maneb 265 C4H6MnN2S4 012427-38-2 90 3 N,N‘ -Bis(pentamethylene)thiuramtetr 384 C12H20N2S6 000000-00-0 56 4 Sulfur, mol. (S8) 256 S8 010544-50-0 55 Abundance Scan 2645 (29.325 min): 4418.D (-) m/ z 63.95 100.00% 64

128 160 5000 256 96 192 TII T T T 29.00 29.20 29.40 29.60 1 TUi • ‘ i ■ • I ■ ■ i ‘ 1 I........... I ' i ' 11"* 224 । । ■ । ■ । । ■ m/z 127.90 53.85% miz-> 60 80 100 120 140 160 180’ 200 220 240 260 Abundance #35240: Sulfur 64 192 128 160 256 5000 96 29.00 29.20 29.40 29.60 ‘ ' 224 m/z 159.85 51.975 I............ ... ■ ■ ■ i ■ • miz-> 60 80 100 ‘ ' 120 140 ' 160 180 * 200 ' 220 ' 240 ~ 260 Abundance #36692 Maneb 64 256 - 102 128 29.00 29.20 29.40 29.60 ' ' ' 5000 160 m/z 255.7 45.15% 192 85 149 212 ■ i ■ ■ ■ ■ i 1 1 1 ‘ i ■ ■ ■ ■ i ■ • ■ ■ i 1 ■ 1 ■ i ■ ■ ■ 1 i ■ ■ 1 ■ i ■ ■ ■ ■ i 1 1 1 1 I 1 1 1 1 I 1 1 miz-> 60 80 100 120 140 160 180 200 220 240 260 Abundance #52456: N,N’-Bis(pentamethylene)thiuramtetrasulfide 64 29.00 29.20 29.40 29.60 ' 192 m/ z 95.80 27.48 128 5000 160 96 224 256 76 11 - i 1 1 1 ' 1 1 i.... I miz-> 60 80 100 120 140 160 180 200 ' ' 220 ' 240 ' ' 260 29.00 29.20 29.40 29.60

4418.D GCMS0308.M Fri Mar 22 09:40:28 2002 Page 4

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