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GCMS analysis results for sample AD29963, Jan 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry report documenting analysis of sample AD29963 conducted on January 28, 2002.

NYC-WTC_000037279–000037288

Folder label: “GCMS X 12/11/01 A 12/18/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1801\29963.D Vial: 10 Acq On : 19 Dec 2001 12:52 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Selenide, ethyl 1-methyl-1-pen Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 25.13 0.27 ug/l 87120 Phenanthrene-d10 24.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual ------------------ -------------------------------------------------- 1 Selenide, et 1 1-methyl-l-penten-3 188 C8H12Se 025128-48-7 47 Anthracene 10- 188 C14D10 001719-06-8 45. CS 3 Cyclohe fione, phenylhydrazone 188 C12H16N2 000946-82-7 28 4 1,4-Na thalenedione, 2-hydroxy-3-m 188 C11H803 000483-55-6 23 Abundance Scan 2188 (25.128 min): 29963.D(.) 18 m/z 188. 10 100 . 00%

5000 80 94 62 118 132 157 24.80 25.00 25.20 25.40 43 54 m/z 79.95 23.82% 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19733: Selenide, ethyl 1-methyl-1-penten-3-ynyl I 1~8

5000 24.80 25.00 25.20 25.40 79 159 m/z 94.00 16.223 145 173

130 140 150 160 170 180 ne-d10- 1

24.80 25.00 25.20 25.40 5000 m/z 18.4.05 14.62;

80 94 160

130 140 150 160 170 180 henylhydrazone

m/z 92.00 11.703

5000 65 77 106 145 159 120 132 170 TT' 100 110 120 130 140 150 160 170 1 24.80 25.00 25.20 25.40

29963.D .GCMS1126.M Tue Jan 15 15:28:53 2002 Page 2

NYC-WTC 000037287

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NYC-WTC_000037287Source: NYC Law Department, mirrored locally

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