NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\MAY1502\LB.D Vial: 3
Acq On : 15 May 2002 4:02 pm Operator:
Sample : GC/MS SCAN 5/10 Inst : 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
Peak Number 3 Sulfur, mol. (S8) Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
29.20 0.83 ug/1 56345 Phenanthrene-dl0 25.54
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Sulfur, mol. (S8) 256 S8 010544-50-0 39
2 N,N’ -Bis(pentamethylene)thiuramtetr 384 C12H20N2S6 000000-00-0 37
3Sulfur dioxide 64 02S 007446-09-5 4
4 Ethyl Chloride 64 C2H5C1 000075-00-3 4
Abundance Scan 2636 (29,199 min): LB.D (-) m/z 63.95 100.00%
64 A
5000
128
160 256
96 -192
28.80 29.00 29.20 29.40 29.60
40 J i 224 -
1 > । > 1 । * 1 ‘ । । ■ ■ ■ i ■ ' 1 1 11 1 1 1 1 1 ' m/z 127.95 38.09%
m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260
Abundance #71623: Sulfur, mol. (S8)
64
5000
192
....... 1
28.80 29.00 29.20 29.40 29.60
128 160 m/z 255.80 31.30%
96
m/z->
48
■ r i ■ ' ' ■ I 1 1 1 1 I
20 40 60
18011.1 4— 7
■ ■ i 1
256
■ ■ i ' '
80 100 120 140 160 .180 200 220 240 260
■ i ■ ■ ■ i t ■ •
Abundance #52456: N,N-Bis(pentamethylene)thiuramtetrasulfide
64
192
128 28.80 29.00 29.20 29.40 29.60
5000 160 m/z 159.90 30.03%
96
256
76 224
- ,l......... i,............. 11 ' ■ ‘ ■ J'1 1 1 1 1 1
rn/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260
Abundance #149: Sulfur dioxide
64 28.80 29.00 29.20 29.40 29.60
m/ Z 95.90 18.81%
A
5000 48
16
m/z—>
— 34—
20 40 60 80 100 120 140 160 180 200 220 240 260 28.80 29.00 29.20 29.40 29.60
LB.D GCMS0510.M Fri May 17 09:16:42 2002 Page 3
NYC-WTC_000024195
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