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GCMS blank analysis results for sample AE10851, May 2002

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Laboratory report showing GCMS blank analysis for sample AE10851 on May 20, 2002, listing compounds below method detection limits.

NYC-WTC_000024187–000024196

Folder label: “GCMS X 5/10/02 A 5/15/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY1502\LB.D Vial: 3 Acq On : 15 May 2002 4:02 pm Operator: Sample : GC/MS SCAN 5/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 3 Sulfur, mol. (S8) Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 29.20 0.83 ug/1 56345 Phenanthrene-dl0 25.54 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Sulfur, mol. (S8) 256 S8 010544-50-0 39 2 N,N’ -Bis(pentamethylene)thiuramtetr 384 C12H20N2S6 000000-00-0 37 3Sulfur dioxide 64 02S 007446-09-5 4 4 Ethyl Chloride 64 C2H5C1 000075-00-3 4 Abundance Scan 2636 (29,199 min): LB.D (-) m/z 63.95 100.00% 64 A

5000 128 160 256 96 -192 28.80 29.00 29.20 29.40 29.60 40 J i 224 - 1 > । > 1 । * 1 ‘ । । ■ ■ ■ i ■ ' 1 1 11 1 1 1 1 1 ' m/z 127.95 38.09% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #71623: Sulfur, mol. (S8) 64

5000 192 ....... 1 28.80 29.00 29.20 29.40 29.60 128 160 m/z 255.80 31.30% 96

m/z-> 48 ■ r i ■ ' ' ■ I 1 1 1 1 I 20 40 60 18011.1 4— 7 ■ ■ i 1 256 ■ ■ i ' ' 80 100 120 140 160 .180 200 220 240 260 ■ i ■ ■ ■ i t ■ •

Abundance #52456: N,N-Bis(pentamethylene)thiuramtetrasulfide 64 192 128 28.80 29.00 29.20 29.40 29.60 5000 160 m/z 159.90 30.03% 96 256 76 224 - ,l......... i,............. 11 ' ■ ‘ ■ J'1 1 1 1 1 1 rn/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #149: Sulfur dioxide 64 28.80 29.00 29.20 29.40 29.60 m/ Z 95.90 18.81% A

5000 48

16

m/z—> — 34— 20 40 60 80 100 120 140 160 180 200 220 240 260 28.80 29.00 29.20 29.40 29.60

LB.D GCMS0510.M Fri May 17 09:16:42 2002 Page 3

NYC-WTC_000024195

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NYC-WTC_000024195Source: NYC Law Department, mirrored locally

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