DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB0802\30708.D Vial: 51 Acq On : 10 Feb 2002 11:46 am Operator: 209 GALOS Sample : GC/MS SCAN 2/8 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Sulfur, mol. (S8) Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

29.45 0.48 ug/1 82800 Phenanthrene-dl0 25.76

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Sulfur, mol. (S8) 256 S8 010544-50-0 39 2 Maneb 265 C4H6MnN2S4 012427-38-2 32 3 N,N‘-Bis(pentamethylene)thiuramtetr 384 C12H20N2S6 000000-00-0 25 4 Sulfu r 256 S8 007704-34-9 11 Abundance Scan 2658 (29.447 min): 30708.D (-) m/z 63.as. ’.. 100.00% 64

5000 128 160 256 -- - 96 192 224 29.20 29.40 29.60 29.80 49 । , 202 - 1 1 ' '' 1 1 i T-r-j-r-r ,i ■ ■ । ■ l - ■ m/z 127.90 38.41% m/Z-2 __ 40 _ _ 60 80 100 120 140 160 180 200 220 240 260 Abundance #71623: Sulfur, mol. (SB) 64

5000 192 * ' I ' 1I‘" 29.20 29.40 29.60 29.80 96 128 160 m/z 255.75 31.67% 48 ■| 2?4 256 m/z->40 1 I ' 11 1 1 60 .8011)011 80 100 120 140___160 1 ■ L ■ ■ <11 I i ‘ i 1 | I 1 1 1 | | ■—r +- [■ i i 180 200 220 240 260 Abundance 13082. Mne 64 ............... /.......................

128 256 29.20 29.40 29.60 29.80 102 5000 160 m/z 159.85 28.61% 192 85 149 212 miz->__ _ 40____ 60.. _.. 80___ 100___ 120 140__ 160 180 200 220 240 260 Abundance #52456: N,N‘-Bis(pentamethylene)thiuramtetrasulfide 64 29.20 29.40 29.60 29.80 192 m/z 95.85 20.08% 128 5000 160 96 76 224 256 ..................... ......................... TI I ' I 1 1 l , 1, , , , , , , 1 I । । । 1 I l'i i 1 । । 1 — 1 1 ' 1 ' ' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 29.20 29.40 29.60 29.80

30708.D GCMS0208.M Thu Feb 14 16:44:39 2002 Page 1

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