GCMS results for sample AE07109, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\1\DATA\APR2402\7109.D Vial: 15 Acq On : 25 Apr 2002 5:23 am Operator: Sample : gc/ms scan 4/23 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Sulfur, mol. (S8) Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

29.25 0.43 ug/1 87040 Phenanthrene-dl0 25.59

Hit# of 5 Tentative ID 256 S8 MW MolForm -------- e CAS# 010544-50-0 95, Qual

1 Sulfur, mol. (S8) 2 Sulfur 256 S8 007704-34-9 $95 3 Maneb 265 C4H6MnN2S4 012427-38-2 78 4 N,N1-Bis(pentamethylene)thiuramtetr 384 C12H20N2S6 000000-00-0 38 Abundance Scan 2637 (29.250 min): 7109.D (-) m/ z 63.90 100.00% 64

128 160 256 5000 96 192

, 224 29.00 29.20 29.40 29.60 44 84 1 —I । ■I . i . . m/z 255.75 55.27% ■ ■ ■ i 1 1 1 1 i

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #35241: Sulfur, mol. (S8) 64 256 128 160 .................... 5000 192 I I t I I I I I I I I

29.00 29.20 29.40 29.60 96 224 m/z 127.80 52.75% 34 1 ' I 1 1 1 ‘ I - I 1 1 ‘ 1 1 1 I— 1.... , ' i 1 1 1 ' 1 1 1 ' 1 1 1 TT 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #35240: Sulfur 64 192 128 160 256 29.00 29.20 29.40 29.60 5000 m/z 159.85 51.77% 96 224

m/z-> ■ ■ 40 i ■ 1 ■ 1 i 60 1......... 80 100 1 120 140 160 180 200 J1' 1 1 i 1 1 220 240 11 260 Abundance #36692: Maneb 1 1 1 i 64 29.00 29.20 29.40 29.60 m/z 191.80 31.74% 128 256 102 5000 160

192 85 149 / I li l 111/t/ttnB I I 1 212 1 1 i ' ' 1 1 i ' 1 i 1 1 ' ‘ I 1 ’ ' **1d—Bn—T f 1 1 I" ’ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 29.00 29.20 29.40 29.60

7109.D GCMS0412.M Thu Apr 25 11:17:13 2002 Page 2

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