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GCMS calibration data for sample AE04388, March 2002

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Calibration record for GCMS analysis of sample AE04388 conducted on March 28, 2002, showing compound responses.

NYC-WTC_000011845–000011848

Folder label: “GCMS X 2/28/02 A 3/26/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR2502\CAL5A.D Vial: 2 Acq On : 25 Mar 2002 1:08 pm Operator : Sample : gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 28 10:27 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Mar 26 14:13:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.22 168 138218 5.52 ug/1 # 81 31) 4-Bromophenyl-phenylether 24.29 248 84259 5.73 ug/1 # 91 32) Hexachlorobenzene 24.73 284 103662 6.07 ug/1 # 86 3 3) Phenanthrene 25.71 178 438528 5.48 ug/1 98 34) Anthracene 25.84 178 414361 5.22 ug/1 99 35) Di-n-butylphthalate 27.61 149 517538 5.14 ug/1 # 98 36) Fluoranthene 29.32 202 418956 4.99 ug/l # 93 3 9) Pyrene 30.00 202 426099 7.32 ug/l # 94 40) Butylbenzylphthalate 32.13 149 183214 6.10 ug/1 # 95 41) Benzo(a)anthracene 33.64 228 246137 5.08 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.91 149 247219 6.10 ug/1 # 95 43) Chrysene 33.77 228 251711 5.30 ug/1 98 45) Di-n-Octylphthalate 35.65 149 311740 6.24 ug/1 # 97 46) Benzo(b)fluoranthene 36.75 252 184909 5.34 ug/1 98 47) Benzo(k)fluoranthene 36.82 252 205310 6.08 ug/1 96 48) Benzo(a)pyrene 37.74 252 141334 4.48 ug/1 # 98 49) Indeno(l,2,3-cd)pyrene 42.06 276 117185 3.08 ug/1 96 50) Dibenz(a,h)anthracene 42.14 278 87308 2.96 ug/1 98 51) Benzo (g,h, Dperylene 43.30 276 103757 3.34 ug/l 96

(#) = qualifier out of range (m) = manual integration CAL5A.D GCMS0308.M Thu Mar 28 10:30:29 2002 Page 2

NYC-WTC_000011847

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NYC-WTC_000011847Source: NYC Law Department, mirrored locally

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