GCMS calibration data for sample AE04388, March 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR2502\CAL5A.D Vial: 2 Acq On : 25 Mar 2002 1:08 pm Operator: Sample : gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 28 10:27 2002 Quant. Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Mar 26 14:13:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.26 152 611152 20.00 ug/1 -0.09 10) Naphthalene-d8 15.89 136 2308761 20.00 ug/1 -0.10 17) Acenaphthene-diO 21.20 164 1263684 20.00 ug/1 -0.11 29) Phenanthrene-diO 25.64 188 1853640 20.00 ug/1 -0.12 38) Chrysene-dl2 33.70 240 1014030 20.00 ug/1 -0.14 44) Perylene-dl2 37.94 264 567015 20.00 ug/1 -0.18

System Monitoring Compounds 37) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = , 0.0 0%

Target Compounds a. 55 Qvalue • 1

2) N-nitroso-dimethyl amine 5.91 74 100919 4.87 ug/1 # 70 3) bis(2-Chloroethyl)ether 11.66 93 180478 5.41 ug/1 89 4) 1,3-Dichlorobenzene 12.16 146 187176 5.42 ug/1 100 5) 1,4-Dichlorobenzene 12.29 146 187194 5.41 ug/1 99 6) 1,2-Dichlorobenzene 12.82 146 175428 5.44 ug/1 99 7) 2,2'-oxybi s(1-Chioropropan 13.13 45 228254 4.86 ug/1 99 8) N-Nitroso-di-n-propylamine 13.53 70 106962 4.92 ug/1 # 86 9) Hexachloroethane 13.66 117 65905 5.10 ug/1 95 11) Nitrobenzene 13.94 77 164797 5.22 ug/1 90 12) 1sophorone 14.58 82 303914 5.08 ug/1 99 13) bis(2-Chloroethoxy)methane 15.26 93 203857 5.20 ug/1 99 14) 1,2,4-Trichlorobenzene 15.77 180 156388 5.77 ug/1 97 15) Naphthalene 15.95 128 480697 5.63 ug/1 99 16) Hexachlorobutadiene 16.49 225 79460 5.88 ug/1 97 18) Hexachlorocyclopentadiene 18.68 237 47417 5.54 ug/1 100 19) 2-Chloronaphthalene 19.46 162 295040 5.44 ug/1 95 20) Dimethylphthalate 20.54 163 338526 5.32 ug/1 98 21) 2,6-Dinitrotoluene 20.75 165 76830 4.98 ug/1 # 82 2 2) Acenaphthylene 20.72 152 417225 5.38 ug/1 98 23) Acenaphthene 21.28 153 301321 5.56 ug/1 98 24) 2,4-Dinitrotoluene 21.93 165 93842 4.54 ug/1 # 74 25) Diethylphthalate 22.68 149 322587 5.23 ug/1 # 94 26) 4-Chlorophenyl-phenylether 22.82 204 158563 6.00 ug/1 91 27) Fluorene 22.81 166 322987 5.63 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.29 77 304619 4.60 ug/L # 84

(#) = qualifier out of range (m) = manual integration CAL5A.D GCMS0308.M Thu Mar 28 10:30:26 2002 Page 1

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