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← Document results/DEP Box 14/GCMS X 2/14/02 A 3/2/02 - 3/20/02
Document / 8 pages

GCMS calibration table for TCLP method, March 2002

Machine-extracted title · confidence 100%

Instrument output displaying calibration data and surrogate recovery results for sample AE03283.

NYC-WTC_000011460–000011467

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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Scanned page image, NYC-WTC_000011463
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C: \HPCHEM\ 1 \DATA\MARO1023283.D Vial: 43 Acq On 3 Mar 2002 5:38 am Operator: Sample gc/ms scan 2/4 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.191 338 343 361 rBV 128789 355044 5.85% 1.195% 2 12.313 786 792 808 rBV 1761547 4270282 70.38% 14.378% 3 15.958 1183 1189 1206 rBV 2466577 5691984 93.81% 19.165% 4 21.273 1761 1768 1786 rBV 2588188 6067582 100.00% 20.430% 5 25.726 2245 2253 2264 rBV2 2457930 5907271 97.36% 19.890%

6 25.854 2264 2267 2281 rVB 29537 88902 1.47% 0.299% 7 30.793 2800 2805 2813 rBV 144980 294727 4.86% 0.992% 8 33.795 3124 3132 3149 rBV2 1602143 4015402 66.18% 13.520% 9 38.073 3587 3598 3623 rBV2 890283 3008285 49.58% 10.129%

Sum of corrected areas: 29699479

3283.D GCMS0208.M Mon Mar 25 12:18:55 2002

NYC-WTC_000011463

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NYC-WTC_000011463Source: NYC Law Department, mirrored locally

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