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← Document results/DEP Box 14/GCMS X 2/14/02 A 3/2/02 - 3/20/02
Document / 8 pages

GCMS calibration table for TCLP method, March 2002

Machine-extracted title · confidence 100%

Instrument output displaying calibration data and surrogate recovery results for sample AE03265.

NYC-WTC_000011407–000011414

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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Scanned page image, NYC-WTC_000011410
OCR text

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C: \HPCHEM\ 1 \DATA\MARO 1023265.D Vial: 40 Acq On 3 Mar 2002 2:39 am Operator: Sample gc/ms scan 2/4 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.186 338 342 351 rBV 126231 308338 5.50% 1.077% 2 12.317 786 792 813 rBV 1649070 3938228 70.26% 13.760% 3 15.962 1182 1189 1206 rBV 2354403 5261424 93.87% 18.383% 4 21.277 1760 1768 1784 rBV 2494098 5605070 100.00% 19.584% 5 25.730 2245 2253 2263 rBV2 2305980 5520158 98.49% 19.287%

6 25.849 2263 2266 2285 rVB 29943 101967 1.82% 0.356% 7 30.797 2799 2805 2814 rBV 143201 293134 5.23% 1.024% 8 33.790 3123 3131 3148 rBV2 1663473 4277492 76.31% 14.945% 9 38.077 3587 3598 3624 rBV2 969734 3315059 59.14% 11.583%

Sum of corrected areas: 28620870

3265.D GCMS0208.M Mon Mar 25 12:16:19 2002

NYC-WTC_000011410

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NYC-WTC_000011410Source: NYC Law Department, mirrored locally

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