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← Document results/DEP Box 14/GCMS X 2/14/02 A 3/2/02 - 3/20/02
Document / 9 pages

GCMS calibration table for TCLP method, March 2002

Machine-extracted title · confidence 100%

Instrument output displaying calibration data and surrogate recovery results for sample AE03381.

NYC-WTC_000011494–000011502

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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Scanned page image, NYC-WTC_000011497
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\MAR0102\3381.D Vial: 45 Acq On 3 Mar 2002 7:37 am Operator: Sample gc/ms scan 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.189 339 343 351 rBV 129167 306632 4.23% 0.845% 2 8.290 351 354 368 rVB 23148 76276 1.05% 0.210% 3 12.320 787 793 814 rBV 2166304 5189203 71.51% 14.292% 4 15.964 1183 1190 1207 rBV 3066533 6832706 94.16% 18.819% 5 21.280 1761 1769 1782 rBV 3142043 7256655 100.00% 19.987%

6 25.732 2245 2254 2264 rBV2 2977447 7161738 98.69% 19.725% 7 25.851 2264 2267 2282 rVB 35830 111470 1.54% 0.307% 8 30.790 2800 2805 2812 rBV 133737 286750 3.95% 0.790% 9 33.802 3123 3133 3151 rBV 1858909 4869760 67.11% 13.413% 10 38.080 3587 3599 3618 rBV2 1220486 4216070 58.10% 11.612%

Sum of corrected areas: 36307260

3381.D GCMS0208.M Mon Mar 25 12:20:48 2002

NYC-WTC_000011497

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NYC-WTC_000011497Source: NYC Law Department, mirrored locally

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