NYC-WTC_000011460
Instrument output displaying calibration data and surrogate recovery results for sample AE03283.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 8 pages
GCMS calibration table for TCLP method, March 2002
Machine-extracted title · confidence 100%Instrument output displaying calibration data and surrogate recovery results for sample AE03384.
NYC-WTC_000011558–000011565Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02”
Page image
OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
LSC Area Percent Report
Data File C:\HPCHEM\l\DATA\MAR0102\3384.D Vial: 48 Acq On 3 Mar 2002 10:35 am Operator: Sample gc/ms scan 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP
If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5
Signal : TIC
peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total
1 8.188 338 343 368 rBV 100345 281935 6.34% 1.246% 2 12.319 787 793 813 rBV 1271347 3120290 70.21% 13.795% 3 15.963 1183 1190 1207 rBV 1783372 4206511 94.66% 18.598% 4 21.269 1761 1768 1781 rBV 1944026 4444040 100.00% 19.648% 5 25.722 2245 2253 2265 rBV2 1871806 4349148 97.86% 19.228%
6 25.860 2265 2268 2277 rVB 23478 60799 1.37% 0.269% 7 30.789 2800 2805 2815 rVB 113215 241410 5.43% 1.067% 8 33.791 3124 3132 3152 rBV 1381904 3383129 76.13% 14.957% 9 38.060 3586 3597 3619 rBV2 749098 2531384 56.96% 11.192%
Sum of corrected areas: 22618646
3384.D GCMS0208.M Mon Mar 25 12:24:00 2002
NYC-WTC_000011561
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NYC-WTC_000011561Source: NYC Law Department, mirrored locally
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1 shared topics · Same agency, volume and box · similarity 0.997
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Technical record of GCMS calibration data for TCLP analysis using sample vial 12 from March 28, 2002.
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