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GCMS analysis results for sample AE02596, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE02596 conducted on March 7, 2002, including surrogate recovery data.

NYC-WTC_000005271–000005280

Folder label: “GCMS X 2/5/02 A 3/1/02

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Scanned page image, NYC-WTC_000005276
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\MAR0102\2596.D Vial: 6 Acq On 1 Mar 2002 1:16 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.197 340 344 352 rBV 12526 27137 1.11% 0.217% 2 12.319 787 793 811 rVB 696651 1676011 68.45% 13.378% 3 15.955 1183 1189 1207 rBV 1022044 2243298 91.62% 17.907% 4 21.270 1761 1768 1788 rBV 1140292 2448461 100.00% 19.544% 5 25.713 2245 2252 2264 rBV2 1001015 2369989 96.80% 18.918%

6 25.851 2265 2267 2278 rVB2 9333 26530 1.08% 0.212% 7 30.790 2800 2805 2815 rBV 139410 286028 11.68% 2.283% 8 33.783 3124 3131 3151 rBV2 784443 1916278 78.26% 15.296% 9 38.061 3588 3597 3623 rBV2 469361 1534016 62.65% 12.245%

Sum of corrected areas: 12527748

2596.D GCMS0208.M Mon Mar 04 11:40:02 2002

NYC-WTC_000005276

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NYC-WTC_000005276Source: NYC Law Department, mirrored locally

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