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GCMS analysis results for sample AE02597, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE02597 conducted on March 7, 2002, including surrogate recovery data.

NYC-WTC_000005281–000005290

Folder label: “GCMS X 2/5/02 A 3/1/02

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Scanned page image, NYC-WTC_000005285
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\MAR0102\2597.D Vial: 7 Acq On 1 Mar 2002 2:15 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.197 340 344 353 rBV 11972 27957 1.16% 0.226% 2 12.310 787 792 809 rVB 659374 1654468 68.53% 13.365% 3 15.955 1183 1189 1206 rBV 1011166 2217441 91.84% 17.912% 4 21.270 1761 1768 1789 rBV 1108132 2414347 100.00% 19.503% 5 25.713 2246 2252 2264 rBV2 1010556 2322601 96.20% 18.762%

6 25.851 2264 2267 2280 rVB2 8926 30901 1.28% 0.250% 7 27.687 2462 2467 2474 rVB 12431 28249 1.17% 0.228% 8 30.790 2800 2805 2814 rVB 136192 287567 11.91% 2.323% 9 33.783 3124 3131 3150 rBV2 801674 1888471 78.22% 15.255% 10 38.052 3587 3596 3612 rBV2 459058 - 1507567 62.44% 12.178%'

Sum of corrected areas: 12379569

2597.D GCMS0208.M Mon Mar 04 11:41:05 2002

NYC-WTC_000005285

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NYC-WTC_000005285Source: NYC Law Department, mirrored locally

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