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← Document results/DEP Box 14/GCMS X 2/14/02 A 3/2/02 - 3/20/02
Document / 8 pages

GCMS calibration table for TCLP method, March 2002

Machine-extracted title · confidence 100%

Instrument output displaying calibration data and surrogate recovery results for sample AE03383.

NYC-WTC_000011539–000011546

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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Scanned page image, NYC-WTC_000011542
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C: \HPCHEM\ 1 \DATA\MAR0102\3383.D Vial: 47 Acq On 3 Mar 2002 9:36 am Operator: Sample gc/ms scan 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 8.185 338 342 361 rBV 69072 199574 4.18% 0.829% 2 12.316 786 792 808 rBV 1380002 3332470 69.81% 13.849% 3 15.961 1182 1189 1205 rBV 1977413 4453570 93.29% 18.508% 4 21.276 1761 1768 1782 rBV 2121513 4773956 100.00% 19.840% 5 25.720 2245 2252 2263 rBV2 1922882 4656552 97.54% 19.352%

6 25.857 2263 2267 2281 rVB 27120 92105 1.93% 0.383% 7 30.796 2800 2805 2814 rVB 89671 188014 3.94% 0.781% 8 33.789 3123 3131 3150 rBV2 1451332 3610166 75.62% 15.003% 9 38.067 3586 3597 3618 rBV2 808660 2756166 57.73% 11.454%

Sum of corrected areas: 24062573

3383.D GCMS0208.M Mon Mar 25 12:23:09 2002

NYC-WTC_000011542

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NYC-WTC_000011542Source: NYC Law Department, mirrored locally

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