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← Document results/DEP Box 14/GCMS X 2/14/02 A 3/2/02 - 3/20/02
Document / 8 pages

GCMS calibration table for TCLP method, March 2002

Machine-extracted title · confidence 100%

Instrument output displaying calibration data and surrogate recovery results for sample AE03281.

NYC-WTC_000011429–000011436

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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Scanned page image, NYC-WTC_000011432
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\MAR0102\3281.D Vial: 41 Acq On 3 Mar 2002 3:39 am Operator: Sample gc/ms scan 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.191 338 343 358 rBV 125938 324759 5.57% 1.104% 2 12.322 787 793 815 rBV 1667639 4054579 69.59% 13.784% 3 15.957 1183 1189 1207 rBV 2347808 5422563 93.07% 18.435% 4 21.273 1761 1768 1787 rBV 2464483 5826087 100.00% 19.807% 5 25.725 2245 2253 2264 rBV2 2361026 5678455 97.47% 19.305%

6 25.854 2264 2267 2277 rVB 27424 79450 1.36% 0.270% 7 30.793 2800 2805 2818 rVB 147139 307606 5.28% 1.046% 8 33.795 3124 3132 3150 rBV2 1715596 4344592 74.57% 14.770% 9 38.073 3586 3598 3624 rBV2 996173 3376215 57.95% 11.478%

Sum of corrected areas: 29414306

3281.D GCMS0208.M Mon Mar 25 12:17:11 2002

NYC-WTC_000011432

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NYC-WTC_000011432Source: NYC Law Department, mirrored locally

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