GCMS analysis results, sample AE02719, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report ’ Data File : C: \MSDCHEM\1\5973N\02FEB28\02719.D Vial: 4 Acq On : 28 Feb 2002 5:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1. . .\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 1,3,5-Cycloheptatriene $$ C... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 4.38 0.04 ug/L 15485 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,3,5-Cycloheptatriene $$ Cycloh... 92 C7H8 000544-25-2 4 2 1,6-Heptadiyne 92 C7H8 002396-63-6 3 3 1,6-Heptadiyne 92 C7H8 002396-63-6 3 4 TRIVINYL BORANE 92 C6H9B 000000-00-0 2 Abundance Scan 89 (4.379 min): 02719.D (-) m/z 91.00 100.00% 91

5000 51 __________ 43 ■ i ■ ■ ■ ■ i ' ' i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ 4.00 4.20 4.40 4.60 4.80 ol • i 1 Thmmmmm 84 —9mmmmmm m/z 92.00 70.70% ।• । 'i ■ • i ■ • ■ ■ i ‘ niz-> 20 25 3035404550556065 70 75 80859095 100 Abundance #5570:1,3,5-Cycloheptatriene $$ Cyclohepta-1,3,5-triene $... 9h

5000 4.00 4.20 4.40 4.60 4.80 65 m/z 51.00 28.81% ,...... . ................................................. .. 0- । । ' ' ■ !■ ' ■ ' I ' ' 'rp-rn-T. ■ . I । A A mfz-> 20253035404550556065 70 75 80859095 100 M N Abundance #5526:1,6-Heptadiyne 91 IJ ", . 4.00 4.20 4.40 4.60 4.80 5000 m/z 43.00 21.63% 27 53 65 37 01 ‘ ■ i ■ ‘ ■ ■ i ■ -rrp- dinjin IpwmOpur '11 ■ ■ “ i1 miz-> 20 25 30 35404550556065 70 75 80859095 100 Abundance #5524: 1,6-Heptadiyne I •' • ‘ I > ■ 91 4.00 4.20 4.40 4.60 4.80 m/z 45.10 17.15% 5000 27 53 65

m/z—> 0 ‘ ■ i “ “ i ■ "I "“il,n 20 25 30 35 40 37 -ll++ - 45 50 55 60 65 70 75 80 85 90 95 100 A 4.00 A I ‘ ' ‘ ■ l ‘ ‘ 1 1 I 1 4.20 4.40 -P 4.60 4.80

02719.D HP022102.M Fri Mar 01 10:07:34 2002 Page 7

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