GCMS analysis results, sample AE02719, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

‘' Data File : C: \MSDCHEM\1\5973N\02FEB28\02719.D Vial: 4 Acq On : 28 Feb 2002 5:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 2-Propenenitrile, 2-chloro-.. Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

4.25 0.10 ug/L 36073 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propenenitrile, 2-chloro- $$ A... 87 C3H2C1N 000920-37-6 4 2 4-0-Methyl-d-arabinose 164 C6H1205 000000-00-0 4 3 Propyl nitrite $$ n-C3H7ONO $$ n... 89 C3H7NO2 000543-67-9 4 4 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 4 Abundance Scan 78 (4.254 min): 02719.D (-) m/z 87.10 100.00% 87 43 55 5000 1 ■ ■ 1 i ‘ ‘ ■ । ■ ■ i ■ • • ■ i • ■ ■ 4.00 4.20 4.40 4.60 0- * • i • * * • 14* •■।•• ■•।। । . । । । । । . rn/z 89.00 83.89% n/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #4298:2-Propenenitrile, 2-chloro- $$ Acrylonitrile, 2-chl... 87

5000 52 4.00 4.20 4.40 4.60 m/z 43.00 77.55% 35 60 47 Il . , ■ '''‘i 0- ... ■ > i • ■ • • i • ■ > i I1t । । । । j ■ ■ I 1' I 1 1 1 1 I 1 1 1 ' I 1 ■ 1 ' i ■ ■ ■ ■ i ' ■ miz-> 30 40 50 60 70 , 80 90 100 110 120 130 Abundance #63795:4-0-Methyl-d-arabinose 87 . 4.00 4.20 4.40 4.60 AAA 5000 m/z 55.10 56.75% 60 45 74 ..... — 100 117 128 0- ' i ■ 1 ■ • i ■ ■ 1 ■ i ■ ■ ■ ■ | • ■ • i * • i * ■ ‘ 1 i ' ■ nz-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #4994: Propyl nitrite $$ n-C3H7ONO $$ n-Propyl nitrite $$ ... 43 “ 4.66 4.20 4.40 4.60 ' m/z 41.10 37.02% 5000

89

■n/z-> 0 1 1 1 1 1 ' 1 i ' 30 40 148,1157,. 7?. |....... 50 60 70 80 90 100 110 120 130 ' 1 ■ ■ ■ ■ i ‘ 1 ■ ■ i ■ ■ ‘ ‘ i ■ 4.00 4.20 4.40 4.60

02719.D HP022102.M Fri Mar 01 10:07:34 2002 Page 6

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