GCMS analysis report for sample AE01636, March 2002

Machine-extracted title · confidence 100%

GCMS laboratory results for sample AE01636 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010086–000010105

Folder label: “GCMS X 1/23/02 A 2/21/02”

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NYC 9/11 Public Portal Document Library Search Compound Report . 'Data File : C : \MSDCHEM\1\5973N\02FEB21\01636 .D Vial: 5 Acq On : 21 Feb 2002 6:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Tricyclo[4.1.0.0(2,7)]hept-... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T.

4.38 0.06 ug/L 24213 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tricyclo[4.1.0.0(2,7)]hept-3-ene... 92 C7H8 035618-58-7 7 2 1,3,5-Cycloheptatriene (CAS) $$ ... 92 C7H8 000544-25-2 7 3 ETHINYLCYCLOPENTENE-(1) 92 C7H8 000000-00-0 7 4 METHYLFULVENE 92 C7H8 000000-00-0 7 Abundance Scan 89 (4.379 min): 01636.D (-) m/z 91.00 100.00% 91

5000

43 85 ■ i ■ ‘ ' 1 i • ■ I ' ‘ ‘ ' I ‘ ‘ ‘ I ‘ . 65 4.00 4.20 4.40 4.60 4.80

m/z-> anip Of ■ • i > • • -1 ‘ i *11 ‘ ‘* i * ■ ■ ■ i1 ■ • * i ■ > ‘ ‘ i ‘ ‘ > i1 • ‘ • i ‘ * • * i ‘ • i ■ 3035404550556065 70 75 80 85 90 95 100 '4 I ‘ *4 ‘ I ‘ ‘ m/z 92.00 53.18% Abundance #5591: Tricyclo[4.1.0.0(2,7)]hept-3-ene (CAS) $$ Homobenzv... 91

5000 4.00 4.20 4.40 4.60 4.80 m/z 43.10 19.67% 65 Of ■ ■ i' ■111 ‘ ■ • ■ i ■ ■1 ■ i' ■ ■ ■ i • ■111'1 ■ ‘ i • ■ ■ ■ 11 •1 ■ i ■ ■ ■ ■ i ■ ■ ‘ ■ i' ■'11 •'1 • i 111111 FrT miz-> 303540 45 50556065 70 75 808590 95 100 Abundance #5568:1,3,5-Cycloheptatriene (CAS) $$ Cycloheptatriene $$... 91 1 i 1 1 ' i ' 1' i 1 4.00 4.20 4.40 4.60 4.80 5000 m/z 85.00 14.37%

39 65 .1 61, । 86 01 ' ■ i' ‘ “ । ‘'111' “ ' i “ ■ ‘ i ‘ ' I'11 ’ I'11' I " “ 11 “ ' I " '' I'' " I " '11 1 ■ i “ ‘11 ■ ■ miz-> 3035404550556065 70 75 808590 95 100 Abundance #5532: ETHINYLCYCLOPENTENE-(1) 91 ■ i'f ■ ■ । ■ ‘ A A 4.00 4.20 4.40 4.60 4.80 m/z 65.10 10.26%

5000

39 0 T‘!——90m/mH**Tt 11pulr TFT 61,65 ■ ‘ i ■ • ' ■ i ■ m/z-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 4.00 4.20 4.40 4.60 4.80

01636.D HP022102 .M Mon Feb 25 10:55:37 2002 Page 6

NYC-WTC_000010095

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NYC-WTC_000010095Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE01637, March 2002 · Box DEP Box 14

NYC-WTC_000010106

GCMS laboratory results for sample AE01637 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

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