NYC-WTC_000010458
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons on February 27, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 7 pages
GCMS calibration table results, February 27-March 19, 2002
Machine-extracted title · confidence 70%Gas chromatography-mass spectrometry calibration analysis with retention times and response values for PAH standards and 2,4-DDD compound detection.
NYC-WTC_000010421–000010427Folder label: “GCMS X 1/27/02 A 2/26/02 - 3/5/02 3/20/02”
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OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report t
Data File : C:\HPCHEM\1\DATA\FEB2502\1964.D Vial: 36 Acq On : 27 Feb 2002 12:26 am Operator: Sample : gc/ms scan 1/29 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
8.20 0.29 ug/ 24671 1,4-Dichlorobenzene-d4 12.32
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 36 2 1,3 -Dioxolane 74 C3H602 000646-06-0 7 3 Formamide, N,N-dimethyl- 73 C3H7NO 000068-12-2 5 4 1-Butanamine, 3-methyl - 87 C5H13N 000107-85-7 5 Abundance Scan 344 (8.198 min): 1964.D (-) m/z 73.00 1 00.00% 73
5000 43 1 l ' ’ ‘ ‘ I ‘ 11 /115 ।।. 7.80 8.00 8.20 8.40 8.60
m/z-> —94 1′1112111109711011111 ,55 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6?, . m/ z ।।111 87 11 ■ ■ > > । • • ■ • । • i • > । • • > < i' 43.05 . 31.61% Abundance #63572: 3-Pentanol, 3-methyl- 73
5000 55 ..... N 7.80 8.00 8.20 8.40 8.60 45 87 m/z 45.05 13.45%
m/z-> 5 27 31 4458. 42 ..j.l.*!....,... I|I I..1 I... । .... । . I.. . . T’I’T 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 84 | 1pp
Abundance #62555: 1,3-Dioxolane 73 7.80 8.00 8.20 8.40 8.60 5000 44 m/z 41.05 12.03% 29 26 1 . | ‘ ■ 11 11 57 68 ■ ■ ■11 ■ ■ ■ ■ i ‘1 ■ ■ i ■ mmmTTTT ■' r ''111 ■111 ■"' i'1 ■11 ■" ■ i ■1 “ i ‘111 miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62527: Formamide. N,N-dimethyl- ■ i • • ‘ ■ i 1 ■ 44 73 7.80 8.00 ' 8.20 8.40 8.60 m/z 71.00 7.12% 5000 30 15
miz-> mm27 384 ttmmp- “'•i” m i11 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 58 . 11 ■ ■111 ■' ■ ■ I ■ ■111 ■ ■ “ 11 7.80 8.00 8.20 8.40 8.60
1964.D GCMS0208.M Tue Mar 19 11:02:27 2002 Page 1
NYC-WTC_000010426
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NYC-WTC_000010426Source: NYC Law Department, mirrored locally
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