GCMS sample analysis results for AE01968, March 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR1902\1968.D Vial: 13 Acq On : 20 Mar 2002 4:46 pm Operator: Sample : gc/ms scan 3/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1-Monolinoleoylglycerol trimet Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

34.97 0.93 ug/1 151437 Chrys ene-d12 33.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monol inoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 37 2 1,1,1,5,7,7,7-Heptamethy1-3,3-bis (t 444 C13H4005Si6 038147-00-1 25 3 Benzoic acid, 2,6-bis [/trimethylsil 370 C16H300Si3 003782-85-2 14 4 3 -1sopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 12 Abundance Scan 3260 (34.970 min): 1968.D (-) m/z 73.00 100.00% 73

5000

45 96 117.. ., 147

■'I 1 1 1*1 i 1 ■■ f 1 1 ' 1 191 221 281 A l,t 325 1 L 355 . 429 491— .. J. „L. 34.60 34.80 35.00 35.20 35.40 m/z 147.00 51.61% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 __________ _____ _______ 5000 147 * 1 * 1 1 ' I ' ‘ 1 ’ I ‘ ‘ ‘ * I ‘ ‘ ‘ * I ' 34.60 34.80 35.00 35.20 35.40 34 103 m/z 221.05 38.37% 281 395 482 ,i, , । i , m/z-> 50 100 ’ 150 '260' '250' '360' 350 400 450 Abundance 73 ■ ‘ i • 147 34.60 34.80 35.00 35.20 35.40 5000 267 m/z 355.05 24.90% 355 429 45 207

m/z—> 50 100 150 200 250 300 350 400 450 Abundance #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trimet 73 355 34.60 34.80 35.00 35.20 35.40 m/z 281.05 22.57% 5000

147 267 47 i li 208 237, r TI m/z-> 50 100 150 200 250 300 350 400 450 34.60 34.80 35.00 35.20 35.40

1968.D GCMS0308.M Thu Mar 21 09:19:15 2002 Page 1

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