GCMS sample analysis results for AE01968, March 2002

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Laboratory report detailing the analytical results for sample AE01968 obtained via GCMS on March 22, 2002.

NYC-WTC_000010359–000010373

Folder label: “GCMS X 1/27/02 A 2/26/02 - 3/5/02 3/20/02”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\l\DATA\MAR1902\1968.D Vial: 13 Acq On : 20 Mar 2002 4:46 pm Operator: Sample : gc/ms scan 3/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Mercaptoacetic acid, bis(trime Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

36.16 3.45 ug/1 381588 Perylene-dl2 37.97

Hit# of 5 Tentative I MW MolForm CAS# Qual

7 1 Mercaptoacetic acid, bis (trimethyls 236 C8H2002SSi 006398-62-5 12 2 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si 000000-00-0 12 3 Silanamine, N- [2,6-dimethyl-4- [ (tri 281 C14H27NOSi 072088-09-6 10 4 Tris(trimethylsily/)borate 278 C9H27BOBSi 004325-85-3 10 Abundance Scan 3390 (36.163 min): 1968.D (-) m/z 100.00% 73 147 5000 221 281 355 ■ ■ l rr ■ i ' ■ ■ ■ i ' ' ' 1 i ' 429

m/z-> 45 I 96 117 .......... 191 249 a4.1 11′0111010311110111100111001113371-0/010231′3310 a 40 60 80 100120140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 AQ14. 35.80 36.00 36.20 36.40 m/z 147.00 55.88% Abundance ............. #30949: Mercaptoacetic acid, bis(trimethylsilyl)- 73 147

_____________ . । . . . . । rm i । ■ ■ ■■■ । T—T" 5000 35.80 36.00 36.20 36.40 221 m/z 221.05 41.40% 45 193 104 ‘i""i TIPTNI-HTITg "i ‘ " r " 'i ■ ■" i" " i' ■" i ■ "■ i' i “ "i ■i' m/z-> 40 60 80 100120140160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance 73 —------ 35.80 36.00 36.20 36.40 147 233 m/z 281.05 24.69% 5000

313 429 189 387 339 11‘11111211117"7111111111110133131711537/1121111/112/111112111121/1111-111311111111111111731 i ■i ‘ m/z->___ 40 60 80 100120140 160180200220240 260280300320340 360 380400420 ------------ Abundance #39584: Silanamine, N-[2,6-dimethyl-4-[(trimethylsily!)oxy] 73 35.80 36.00 36.20 36.40 281 m/z 355.0 23.01% 209 5000 251 45 . 179 ------- 125 147..1, IBt-rnumrrT 'i‘" ■ i11 “i11 i । i । i i । i i ( i । । ir n । । i । । m/z-> 40 60 80 100120140160180200220240 260280 300320340 360380400420 35.80 36.00 36.20 36.40

1968.D GCMS0308.M Thu Mar 21 09:19:19 2002 Page 2

NYC-WTC_000010367

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