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GCMS calibration table for TCLP analysis, Feb 13, 2002

Machine-extracted title · confidence 90%

Calibration table listing internal standards and response factors for GCMS Method 508.

NYC-WTC_000009554–000009556

Folder label: “GCMS X 1/14/02 A 3/4/02

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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\FEB1102\REFC.D Vial: 44 Acq On : 13 Feb 2002 5:58 am Operator: 209 GALOS Sample : GC/MS SCAN 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 13 6:47 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Feb 08 15:29:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.32 168 21022 98 (1:63 ug/] 31) 4-Bromophenyl-phenylether 24.41 248 17295 C2.08ug/1 98 32) Hexachlorobenzene 24.84 284 20578 211ug/1 98 3 3) Phenanthrene 25.82 178 93636 C2.30ug/1 100 3 4) Anthracene 25.95 178 78511 (2.02 ug/l 99 35) Di-n-butylphthalate 27.72 149 134897 2.43 ug/l 99 36) Fluoranthene 29.45 202 87820 (2.21 ug/1 100 39) Pyrene 30.13 202 91851 (2.2) ug/l 99 40) Butylbenzylphthalate 32.26 149 30841 (.34 ug/1 95 41) Benzo(a)anthracene 33.77 228 66524 2.19 ug/1 98 42) Bis(2-ethylhexyl)phthalate 34.03 149 43154 (1.39 ug/l 97 43) Chrysene 33.89 228 79639 (2.66 ug/1 98 45) Di-n-Octylphthalate 35.77 149 36667 0.76' ug/1 # 94 46) Benzo(b)fluoranthene 36.89 252 51596 1.89 ug/1 97 47) Benzo(k)fluoranthene 36.96 252 67139 C2.45 ug/1 96 4 8) Benzo(a)pyrene 37.90 252 37825 1.67ug/1 94 49) Indeno(1,2,3-cd)pyrene 42.34 276 35213 C1.71uq/l 96 50) Dibenz(a,h)anthracene 42.40 278 30916 1.96ug/1 98 51) Benzo(g,h,i)perylene 43.59 276 35339 (2.12 ug/1 99

(#) = qualifier out of range (m) = manual integration REFC.D GCMS0208.M Wed Feb 20 12:01:43 2002 Page 2

NYC-WTC_000009555

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NYC-WTC_000009555Source: NYC Law Department, mirrored locally

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