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GCMS analysis results for sample AE02966, February 2002

Machine-extracted title · confidence 100%

Laboratory report for DEP sample AE02966 listing concentrations of target compounds including nitrosamines and chlorobenzenes.

NYC-WTC_000005610–000005613

Folder label: “GCMS X 2/7/02 A 2/9/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\FEB0 80 2\CAL4 0A.D Vial: 27 Acq On 9 Feb 2002 10:36 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 13 9:53 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Feb 08 15:29:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.36 168 845479 38.11 ug/1 95 31) 4-Bromophenyl-phenylether 24.42 248 561026 39.12 ug/1 98 3 2) Hexachlorobenzene 24.86 284 657079 39.12 ug/1 99 33) Phenanthrene 25.85 178 2721600 39.77 ug/1 100 34) Anthracene 25.97 178 2627224 39.18 ug/1 100 35) Di-n-butylphthalate 27.74 149 3839431 40.14 ug/1 100 36) Fluoranthene 29.47 202 2821120 41.29 ug/1 95 3 9) Pyrene 30.15 202 2872196 38.51 ug/1 95 40) Butylbenzylphthalate 32.27 149 1532991 37.12 ug/1 98 41) Benzo(a)anthracene 33.79 228 2202994 40.40 ug/1 100 42) Bis(2-ethylhexyl)phthalate 34.03 149 1970534 35.33 ug/1 99 43) Chrysene 33.92 228 2121459 39.54 ug/1 99 45) Di-n-Octylphthalate 35.78 149 2909398 34.79 ug/1 99 46) Benzo(b)fluoranthene 36.93 252 1869238 39.61 ug/1 99 47) Benzo(k)fluoranthene 37.00 252 1835645 38.71 ug/1 99 4 8) Benzo(a)pyrene 37.95 252 1571800 40.18 ug/1 99 49) Indeno(l,2,3-cd)pyrene 42.39 276 1494253 41.86 ug/1 99 50) Dibenz(a,h)anthracene 42.45 278 1164950 42.70 ug/1 99 51) Benzo(g,h,i)perylene 43.67 276 1173960 40.79 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL4 0A.D GCMS0208.M Wed Feb 13 09:54:18 2002 Page 2

NYC-WTC_000005612

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NYC-WTC_000005612Source: NYC Law Department, mirrored locally

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