GCMS Method 508 data table, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\FEB1102\LBB.D Vial: 30 Acq On : 12 Feb 2002 4:21 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.23 0.59 ug/1 44503 1,4-Dichlorobenzene-d4 12.35

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 Silane/ tetramethyl- 88 C4H12Si 000075-76-3 9 4 Pentane, 3-methoxy-_ _______ 102 C6H140 _ 036839-67-5 9 Abundance 6 Scan 347 (8.226 min): LBB.D (-) m/ z 73.00 1100.00% 73

5000 43 TT-rT-n-p-r-r-rT-T-n-T-n-T-rT-T-T-yn^ 7.80 8.00 8.20 8.40 8.60 . ■ i “ •' i ■1 ‘ ■ i ‘ ..• | 84“ J H87J I | H ■ i “' ■ i “ “ I ■'1' i 447,51.55,59. *1| • • • 35 39 ..J I | I 1 m/ z 43.05 38.78% m/z->__ 5 10 .. 15 20 25 30 .. 35 .. 40 45 50.. 55 60 65 70 75 80 85 90 95 Abundance #63572: 3-Pentanol,3-methyl- 73

5000 55 7.80 8.00 8.20 M....8.40 8.60 45 87 m/ Z 45.05 13.12% 27 31 42 69 84 | 59 Tpmmmhppmptm T’II’TT II ■'! I' 1 " I "‘'l. . m/z->___ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75_.80_85 90 95 Abundance i ~............. .. 30

7.80 8.00 8.20 8.40 8.60 5000 m/z ( 10.69

15 27 70 4144 5558 87 10110001110011—002000puua—nmmuuugggT m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #845: Silane, tetramethyl- 73 7.80 8,00 8.20 8.40 8.60 m/z 74.00 6.83 5000

45 *—152nutn —2m031—n—mnm—42 ______ 59 । 55 tammmmm*aaTg ——ma— 88 1***I** m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8.20 8.40 8.60

LBB.D GCMS0208.M Wed Feb 20 09:56:18 2002 Page 1

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