Laboratory data table recording drip rates and volumes for GCMS Method 508 analysis.
NYC-WTC_000009428–000009436Folder label: “GCMS X 1/14/02 A 2/25-2/26”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\FEB1102\LBB.D Vial: 30 Acq On : 12 Feb 2002 4:21 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/14 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Methoxychlor Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
33.72 0.60 ug/1 45747 Chrysene-dl2 33.82
Hit# of 5 Tentative ID MW MolForm CAS# Qual
<1 Methoxychlor 344 C16H15C13O2 000072-43-5 90 2 Phenol, 4-[[(4-methoxyphenyl)methyl 227 C14H13NO2 003230-39-5 64 3 Benzoic acid, 3-(phenylamino)-, met 227 C14H13NO2 055622-43-0 42 4 S-Indacene, 1,2,3,5,6,7-hexahydro-l 242 C18H26 017465-58-6 38 Abundance Scan 3124 (33.720 min): LBB.D (-) m/z 227.10 100.00% 227
5000 . ... 36 63 89 113 132, 152 169 196 212 274 33.40 33.60 33.80 34.00 ------ ■ ‘ | ‘ i '1 1‘ I ‘ '“ ! ' "•I‘ 1 m/z 228.00 .14.86% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73611: Methoxychlor 227
5000 33.40 33.60 33*80 34.00 ‘ m/z 152.00 10.79% 35 61 114 152 169 196 212 274 mnpmnmp] . .'|.... 111।।j.... 344 t., miz->___ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance 29252: PAnc, . ■ mmdnyenelemingf 227 1 1 1 1 ■ ■ ■ 1 ■ • 1 ■ 1 1 1 1 1 1 1 1 1 1 1 33.40 33.60 33.80 34.00 5000 m/z 153.00 6.40% 65 1 93 120 154 183 211
miz-s 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #29342: Benzoic acid, 3-(phenyiamino)-, methyl ester 227 33.40 33.60 33.80 34'00 ' m/z 169.00 6.34% 5000 167 N 196
m/z—> ■ ■ i " •' i1 40 60 .77,1298,111/1.138.11// I * ‘' * I ‘ ' ‘ I “ • * I “ • ‘ I ‘‘ ‘ I • “ ‘ I “ “ I “ 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ‘ ‘ I ‘ **118 33.40 33.60 33.80 34.00 ‘ ‘ l ‘ ‘ ‘ 1 I
LBB.D GCMS0208.M Wed Feb 20 09:56:29 2002 Page 2
NYC-WTC_000009435
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