GCMS analysis results for sample AD30013, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1801\30013.D Vial: 8 Acq On : 18 Dec 2001 10:55 pm Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1,l-Dichloro-2,2-bis(p-chlorop Concentration Rank 3

R.T. EstCone Area Relative to ISTD R.T.

30.06 3.03ug/l 664/62 Chrysene - dl2 33.01

Hit# of 5 Tentative MW MolForm CAS# Qual 1 1,l-Dichloro-2,2-bi TO enyl 318 C14H10C14 000072-54-8 94 2 Mitotane 318 C14H10C14 000053-19-0-90 3 Chlorophenothane 352 C14H9C15 000050-29-3 72 4 Methyl bis(p-chloropheny acetate 294 C15H12C12O2 005359-38-6 50 Abundance■ Scan 2725 (30.058 mim): 30013.D (-) m/z 234.95 100.00% \ 235

165 5000 199 Ji ■ \' ________ 1 ■ i ■ ' ■ ■ i ■ ■ 29.80 30.00 30.20 30.40

m/z--> ,26.51417411 +A-A 184 1 214 40 60 122137 p i -rt | ’ . o p 1-Tr | r, I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 250 283 320 I T I I | I | I | | I I " I " "‘I " " I " ' ■ I, m/z 236.95 62.95% Abundance #73201: 1,1-Dichloro-2,2-bis(p-chlorophenyl)ethane 235-

/ 5000 165 TIT 29.80 30.00 30.20 30.40 199 m/ z 165.00 58.58% 101 137 rmn T A— TTTTTTT’T ’ I ■ i' ■ ‘ ■ i " u P T’TT 322 TTTTT T‘ m/z-> 40 60 80 100 120 14 160 180 200 220 240 260 280 300 320 340 Abundance #73208: Mitotane 235 i / — 1 29.80 30.00 30.20 30.40 5000 165 m/z 198.95 20.70% 199 L 214 286 320 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73698: Chlorophenothane ) i TU" 235 29.80 30.00 30.20 30.40__ m/z 235.95 15.82% 5000 165 88 199

m/z-> 35

40 60 PmPPP — 4214 +281 TT 80 100 120 140 160 180 200 220 240 260 280 300 320 340 354 ... 4... ' 29.80 30.00 30.20 30.40

30013.D GCMS1126.M Tue Jan 15 15:34:40 2002 Page 6

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