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← Document results/DEP Box 16/GCMS X 12/18/01 A 12/30/01
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GCMS blank analysis results for sample AD30643, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.

NYC-WTC_000018420–000018435

Folder label: “GCMS X 12/18/01 A 12/30/01”

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Scanned page image, NYC-WTC_000018434
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC27O1\LBE.D Vial: 51 Acq On : 30 Dec 2001 8:17 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 1,l-Dichloro-2,2-bis(p-chlorop Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

30.07 2.57 ug/1 717294 Chrysene-dl 2 33.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual __________ ----------------------------------------------------------------------- 1 1,1-Diehl 2,2-bis(p- chlorophenyl 318 C14H10C14 000072-54-8 95 2 Mitotane 318 C14H10C14 000053-19-0 87 3 Technical chlorophenothane 704 C28H18C110 008017-34-3 64 4 ChloroghemethaneScan 2726 (30.069 min): LBE.D (-) t 352 C14H9C15 000050-29-3 64 Abundance m/z 234.95 100.00% 235 165 5000 ................ .......................... 199 2 50 J 88 101 ,4137151,178 212 29.80 30.00 30.20 30.40

mlz-> 14,74 320 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 248 284 • 1 » I I < I I > I I I I » I I I » •)' > m/z 236.95 65.20% Abundance #73201:1,1-Dichloro-2,2-bis(p-chlorophenyl)ethane 235

5000 165 T l • ‘ • l • • 29.80 30.00 30.20 30.40 m/z 165. CIO 59.76% _______________101 178 199212 miz-> I_____ ’ • l • ‘ “ I • ’ ‘ ‘ I ‘ ‘ ‘ ’ i* ‘1 ‘ I ’ 40 60 ?*e 80 100 120 140 160 180 200 220 240 260 280 300 320 tt+t-j-tt |_________________ 322 15444144**

Abundance #73208; Mitotane 235

29.80 30.00 30.20 30.40 5000 165 20.89%

■ TI 199 178 I 212 •' i ■ ■ ■ • i ■ ■ ■ ■ i" • ■ i ■ • ■ • i • ■ ■ ■ i ■ ■ ■ ■ i • TH 248 286 320 11WWMILOTRTTRTTIT miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #61666: Technical chlorophenothane 11** 165 235 29.80 30.00 30.20 30.40 m/z 75.00 16.38% 5000 75 88 199 ,106 123^ .

m/z—> 35 ■ ■i■■■■i • •• • i ■ 40 60 HLa 80 100 120 140 160 180 200 220 240 260 280 300 320 | 212 । 1111111111 i'i । ■! ' “ 111' 1 111 । " I " ... y rr ... 29.80 30.00 30.20 30.40

LBE.D GCMS1126.M Fri Feb 01 11:32:09 2002 Page 9

NYC-WTC_000018434

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NYC-WTC_000018434Source: NYC Law Department, mirrored locally

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Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.994

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