Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
NYC-WTC_000018420–000018435Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC27O1\LBE.D Vial: 51 Acq On : 30 Dec 2001 8:17 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 1,l-Dichloro-2,2-bis(p-chlorop Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.
30.07 2.57 ug/1 717294 Chrysene-dl 2 33.03
Hit# of 5 Tentative ID MW MolForm CAS# Qual __________ ----------------------------------------------------------------------- 1 1,1-Diehl 2,2-bis(p- chlorophenyl 318 C14H10C14 000072-54-8 95 2 Mitotane 318 C14H10C14 000053-19-0 87 3 Technical chlorophenothane 704 C28H18C110 008017-34-3 64 4 ChloroghemethaneScan 2726 (30.069 min): LBE.D (-) t 352 C14H9C15 000050-29-3 64 Abundance m/z 234.95 100.00% 235 165 5000 ................ .......................... 199 2 50 J 88 101 ,4137151,178 212 29.80 30.00 30.20 30.40
mlz-> 14,74 320 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 248 284 • 1 » I I < I I > I I I I » I I I » •)' > m/z 236.95 65.20% Abundance #73201:1,1-Dichloro-2,2-bis(p-chlorophenyl)ethane 235
5000 165 T l • ‘ • l • • 29.80 30.00 30.20 30.40 m/z 165. CIO 59.76% _______________101 178 199212 miz-> I_____ ’ • l • ‘ “ I • ’ ‘ ‘ I ‘ ‘ ‘ ’ i* ‘1 ‘ I ’ 40 60 ?*e 80 100 120 140 160 180 200 220 240 260 280 300 320 tt+t-j-tt |_________________ 322 15444144**
Abundance #73208; Mitotane 235
29.80 30.00 30.20 30.40 5000 165 20.89%
■ TI 199 178 I 212 •' i ■ ■ ■ • i ■ ■ ■ ■ i" • ■ i ■ • ■ • i • ■ ■ ■ i ■ ■ ■ ■ i • TH 248 286 320 11WWMILOTRTTRTTIT miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #61666: Technical chlorophenothane 11** 165 235 29.80 30.00 30.20 30.40 m/z 75.00 16.38% 5000 75 88 199 ,106 123^ .
m/z—> 35 ■ ■i■■■■i • •• • i ■ 40 60 HLa 80 100 120 140 160 180 200 220 240 260 280 300 320 | 212 । 1111111111 i'i । ■! ' “ 111' 1 111 । " I " ... y rr ... 29.80 30.00 30.20 30.40
LBE.D GCMS1126.M Fri Feb 01 11:32:09 2002 Page 9
NYC-WTC_000018434
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NYC-WTC_000018546
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019049
Laboratory report documenting gas chromatography-mass spectrometry blank analysis for volatile organic compounds conducted on January 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017663
Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017126
Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034958
Calibration report showing recovery percentages for various chemical standards used in the GCMS analysis.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004149
Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036798
GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035776
Laboratory data sheet recording GCMS analysis of a blank sample for nitrosamines and chlorinated compounds.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031088
Gas chromatography-mass spectrometry analysis of environmental sample AD26202 conducted Dec 5, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.993
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
Filed in the same folder
NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
Filed in the same folder
NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
Filed in the same folder